N⁽¹⁾-(4-butylphenyl)-N⁽²⁾-(3-(hydroxymethyl)phenyl)-N⁽¹⁾,N⁽²⁾-dimethylphthalamide

Base Information

• Chemical Name: N⁽¹⁾-(4-butylphenyl)-N⁽²⁾-(3-(hydroxymethyl)phenyl)-N⁽¹⁾,N⁽²⁾-dimethylphthalamide
• CAS No.: 1361226-21-2
• Molecular Formula: C₂₇H₃₀N₂O₃
• Molecular Weight: 430.547

Synonyms:N⁽¹⁾-(4-butylphenyl)-N⁽²⁾-(3-(hydroxymethyl)phenyl)-N⁽¹⁾,N⁽²⁾-dimethylphthalamide

Chemical Property of N⁽¹⁾-(4-butylphenyl)-N⁽²⁾-(3-(hydroxymethyl)phenyl)-N⁽¹⁾,N⁽²⁾-dimethylphthalamide

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Technology Process of N⁽¹⁾-(4-butylphenyl)-N⁽²⁾-(3-(hydroxymethyl)phenyl)-N⁽¹⁾,N⁽²⁾-dimethylphthalamide

There total 1 articles about N⁽¹⁾-(4-butylphenyl)-N⁽²⁾-(3-(hydroxymethyl)phenyl)-N⁽¹⁾,N⁽²⁾-dimethylphthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N(1)-(4-butylphenyl)-N(1),N(2)-dimethyl-N(2)-(3-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)phthalamide (1361226-03-0) → N(1)-(4-butylphenyl)-N(2)-(3-(hydroxymethyl)phenyl)-N(1),N(2)-dimethylphthalamide (1361226-21-2)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; at 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201102018

Reference yield: 66.0%

N(1)-(4-butylphenyl)-N(2)-(3-(hydroxymethyl)phenyl)-N(1),N(2)-dimethylphthalamide (1361226-21-2) + (S)-(1,1'-binaphthyl-2,2'-dioxy)chlorophosphine → N(1)-(4-butylphenyl)-N(2)-(3-(((11bS)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yloxy)methyl)phenyl)-N(1),N(2)-dimethylphthalamide

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201102018

upstream raw materials:

N⁽¹⁾-(4-butylphenyl)-N⁽¹⁾,N⁽²⁾-dimethyl-N⁽²⁾-(3-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenyl)phthalamide

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