C₂₂H₂₆O₅S

Base Information

• Chemical Name: C₂₂H₂₆O₅S
• CAS No.: 1352496-70-8
• Molecular Formula: C₂₂H₂₆O₅S
• Molecular Weight: 402.511
• Mol file: 1352496-70-8.mol

Synonyms:C₂₂H₂₆O₅S

Chemical Property of C₂₂H₂₆O₅S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₆O₅S

There total 3 articles about C₂₂H₂₆O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C25H32O4S3 (1352496-96-8) → C22H26O5S (1352496-70-8)

Guidance literature:

With water; calcium carbonate; methyl iodide; In acetonitrile; at 40 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2011.09.011

Reference yield:

C16H24O3S2 (1352496-66-2) → C22H26O5S (1352496-70-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethylmagnesium bromide; lithium chloride / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: water; calcium carbonate; methyl iodide / acetonitrile / 40 °C / Inert atmosphere

With ethylmagnesium bromide; water; calcium carbonate; lithium chloride; methyl iodide; In tetrahydrofuran; diethyl ether; acetonitrile;

DOI:10.1016/j.tet.2011.09.011

Reference yield:

(2S)-2-[2-(4-methoxyphenoxy)ethyl]-2-methyloxirane (603961-40-6) → C22H26O5S (1352496-70-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -20 °C / Inert atmosphere

1.2: -20 - 20 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: ethylmagnesium bromide; lithium chloride / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

3.1: water; calcium carbonate; methyl iodide / acetonitrile / 40 °C / Inert atmosphere

With n-butyllithium; ethylmagnesium bromide; water; calcium carbonate; lithium chloride; methyl iodide; In tetrahydrofuran; diethyl ether; hexane; acetonitrile;

DOI:10.1016/j.tet.2011.09.011

upstream raw materials:

C₁₆H₂₄O₃S₂

C₂₅H₃₂O₄S₃

(2S)-2-[2-(4-methoxyphenoxy)ethyl]-2-methyloxirane

Downstream raw materials:

C₂₂H₂₈O₅S

C₂₉H₃₁NO₈S

C₂₂H₂₈O₅S

C₂₈H₄₂O₅SSi