2'-(N-tert-butyloxycarbonylaminomethyl)-4'-carboxymethyl-6'-(N⁶-benzoyladenine-9-yl)morpholine

Base Information

• Chemical Name: 2'-(N-tert-butyloxycarbonylaminomethyl)-4'-carboxymethyl-6'-(N⁶-benzoyladenine-9-yl)morpholine
• CAS No.: 1355614-02-6
• Molecular Formula: C₂₄H₂₉N₇O₆
• Molecular Weight: 511.538

Synonyms:2'-(N-tert-butyloxycarbonylaminomethyl)-4'-carboxymethyl-6'-(N⁶-benzoyladenine-9-yl)morpholine

Chemical Property of 2'-(N-tert-butyloxycarbonylaminomethyl)-4'-carboxymethyl-6'-(N⁶-benzoyladenine-9-yl)morpholine

Chemical Property:

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Technology Process of 2'-(N-tert-butyloxycarbonylaminomethyl)-4'-carboxymethyl-6'-(N⁶-benzoyladenine-9-yl)morpholine

There total 5 articles about 2'-(N-tert-butyloxycarbonylaminomethyl)-4'-carboxymethyl-6'-(N⁶-benzoyladenine-9-yl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

di-tert-butyl dicarbonate (24424-99-5) + 2'-aminomethyl-4'-carboxymethyl-6'-(N6-benzoyladenine-9-yl)morpholine (1355613-98-7) → 2'-(N-tert-butyloxycarbonylaminomethyl)-4'-carboxymethyl-6'-(N6-benzoyladenine-9-yl)morpholine (1355614-02-6)

Guidance literature:

With sodium hydroxide; In isopropyl alcohol; at 20 - 60 ℃;

DOI:10.1134/S1068162011060070

Reference yield:

C17H14N8O4 → 2'-(N-tert-butyloxycarbonylaminomethyl)-4'-carboxymethyl-6'-(N6-benzoyladenine-9-yl)morpholine (1355614-02-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: triethylamine / water; ethanol / 1 h / pH 9 - 9.5

1.2: 2.5 h

2.1: 4% Pd/C; hydrogen / ethanol / 48 h

3.1: sodium hydroxide / isopropyl alcohol / 20 - 60 °C

With 4% Pd/C; hydrogen; triethylamine; sodium hydroxide; In ethanol; water; isopropyl alcohol;

DOI:10.1134/S1068162011060070

Reference yield:

2'-azidomethyl-4'-carboxymethyl-6'-(N6-benzoyladenine-9-yl)morpholine (1355613-94-3) → 2'-(N-tert-butyloxycarbonylaminomethyl)-4'-carboxymethyl-6'-(N6-benzoyladenine-9-yl)morpholine (1355614-02-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 4% Pd/C; hydrogen / ethanol / 48 h

2: sodium hydroxide / isopropyl alcohol / 20 - 60 °C

With 4% Pd/C; hydrogen; sodium hydroxide; In ethanol; isopropyl alcohol;

DOI:10.1134/S1068162011060070

upstream raw materials:

2'-azidomethyl-4'-carboxymethyl-6'-(N⁶-benzoyladenine-9-yl)morpholine

di-tert-butyl dicarbonate

2'-aminomethyl-4'-carboxymethyl-6'-(N⁶-benzoyladenine-9-yl)morpholine

N-benzoyladenosine

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