Technology Process of C19H20INO6
There total 4 articles about C19H20INO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C21H25NO6;
With
potassium hydroxide;
In
ethanol; water;
at 120 ℃;
for 2h;
With
iodine; sodium hydrogencarbonate;
In
water;
at 20 ℃;
for 4h;
DOI:10.1021/ol3027945
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 °C
2.1: triethylamine / dichloromethane / 2 h / 0 °C
3.1: caesium carbonate / N,N-dimethyl-formamide / 20 h / 100 °C
4.1: potassium hydroxide / water; ethanol / 2 h / 120 °C
4.2: 4 h / 20 °C
With
sodium hydrogencarbonate; caesium carbonate; triethylamine; potassium hydroxide;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol3027945
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 20 h / 100 °C
2.1: potassium hydroxide / water; ethanol / 2 h / 120 °C
2.2: 4 h / 20 °C
With
caesium carbonate; potassium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol3027945