14-[4-[2-(tert-butyloxycarbonyl)-3-acetyl-guanidino-methyl]-benzyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester

Base Information

Chemical Name:14-[4-[2-(tert-butyloxycarbonyl)-3-acetyl-guanidino-methyl]-benzyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester
CAS No.:1221569-55-6
Molecular Formula:C₃₈H₅₄N₄O₁₃
Molecular Weight:774.866
Hs Code.:

14-[4-[2-(tert-butyloxycarbonyl)-3-acetyl-guanidino-methyl]-benzyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester

Synonyms:14-[4-[2-(tert-butyloxycarbonyl)-3-acetyl-guanidino-methyl]-benzyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester

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Chemical Property of 14-[4-[2-(tert-butyloxycarbonyl)-3-acetyl-guanidino-methyl]-benzyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester

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Technology Process of 14-[4-[2-(tert-butyloxycarbonyl)-3-acetyl-guanidino-methyl]-benzyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester

There total 1 articles about 14-[4-[2-(tert-butyloxycarbonyl)-3-acetyl-guanidino-methyl]-benzyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 204584-80-5
tert-butyl (acetamido(methylthio)methylene)carbamate

: 14-[((4-aminomethyl)phenyl)methyl-amino]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester dihydrochloride

: 1221569-55-6
14-[4-[2-(tert-butyloxycarbonyl)-3-acetyl-guanidino-methyl]-benzyl]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester

Guidance literature:: 14-[((4-aminomethyl)phenyl)methyl-amino]-6,7,9,10,13,14,15,16,18,19,21,22-dodecahydro-12H-5,8,11,17,20,23-hexaoxa-14-aza-benzocycloheneicosene-2,3-dicarboxylic acid dimethyl ester dihydrochloride; With triethylamine; In chloroform; at 20 ℃; for 0.333333h;

tert-butyl (acetamido(methylthio)methylene)carbamate; In chloroform; at 40 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.01.028