[(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)Cr(THF)2]

Base Information

Chemical Name:[(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)Cr(THF)2]
CAS No.:1333117-63-7
Molecular Formula:C₄₀H₅₈CrN₂O₂
Molecular Weight:650.909
Hs Code.:

Synonyms:[(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)Cr(THF)2]

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Chemical Property of [(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)Cr(THF)2]

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Technology Process of [(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)Cr(THF)2]

There total 3 articles about [(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)Cr(THF)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: chromium dichloride

: 500876-61-9
(Li₂(N,N'-[1,3-phenylenebis(methylene)]bis-2,6-diisopropylaniline(-2H)))2

: 1333117-63-7
[(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)Cr(THF)2]

Guidance literature:: In tetrahydrofuran; at -80 - 20 ℃; Schlenk technique; Inert atmosphere;

Reference yield: 10.0%

: [CrCl₂Me(tetrahydrofuran)3]

: 500876-61-9
(Li₂(N,N'-[1,3-phenylenebis(methylene)]bis-2,6-diisopropylaniline(-2H)))2

: 1333117-63-7
[(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)Cr(THF)2]

: 1333117-62-6
[chromium(IV)(methyl)(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)(THF)]

Guidance literature:: In diethyl ether; at -80 - 20 ℃; Schlenk technique; Inert atmosphere;

Reference yield: 10.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: chromium dichloride

: 500876-61-9
(Li₂(N,N'-[1,3-phenylenebis(methylene)]bis-2,6-diisopropylaniline(-2H)))2

: 1333117-63-7
[(2,6-bis(([2,6-bis(1-methylethyl)phenyl]azanidyl)methyl)phenyl)Cr(THF)2]

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; Schlenk technique; Cr compd. (2 equiv.) was added with stirring to soln.of ligand in THF at -80°C; warmed to room temp.; stirred for 1 h; evapd. (vac.); dissolved in pentane; filtered; evapd. (vac.); dissolved in ether; cooled to -35°C; elem. anal.;
DOI:10.1021/om200547u