methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside
CAS No.:1245566-92-0
Molecular Formula:C₃₇H₃₈N₁₀O₁₀
Molecular Weight:782.77
Hs Code.:

methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

Synonyms:methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

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Chemical Property of methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

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Technology Process of methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

There total 12 articles about methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1245566-90-8
methyl 2,6-diazido-2,6-dideoxy-3-O-benzyl-β-D-glucopyranoside

: 1245566-84-0
phenyl 4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-1-thio-β-D-glucopyranoside

: 1245566-92-0
methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

Reference yield: 53.0%

: 1245566-90-8
methyl 2,6-diazido-2,6-dideoxy-3-O-benzyl-β-D-glucopyranoside

: 1245566-84-0
phenyl 4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-1-thio-β-D-glucopyranoside

: 1245566-92-0
methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

: 1379976-86-9
C₃₇H₃₈N₁₀O₁₀

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at 0 ℃; for 1h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo200951p

Reference yield:

: 1245566-89-5
C₁₅H₂₁N₃O₇S

: 1245566-92-0
methyl (4-O-acetyl-2-azido-2-deoxy-3-O-benzyl-6-deoxy-6-phthalimido-α-D-glucopyranosyl)-(1->4)-2,6-diazido-2,6-dideoxy-3-O-benzyl-α-D-glucopyranoside

: 1379976-86-9
C₃₇H₃₈N₁₀O₁₀

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 10.5 h / 80 °C / Inert atmosphere

2: N-iodo-succinimide; trifluorormethanesulfonic acid / diethyl ether; dichloromethane / 1 h / 0 °C / Inert atmosphere

With N-iodo-succinimide; sodium azide; trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo200951p