10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

Base Information

Chemical Name:10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion
CAS No.:86814-89-3
Molecular Formula:C₁₆H₁₃N₃O₂
Molecular Weight:279.298
Hs Code.:

10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0<sup>2,6</sup>>undec-8-en-3,5-dion

Synonyms:10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

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Chemical Property of 10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

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Technology Process of 10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

There total 5 articles about 10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 86814-84-8
(10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

: 86814-89-3
10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; for 0.0833333h; Ambient temperature;

Reference yield:

: 4233-33-4
4-Phenyl-1,2,4-triazolidine-3,5-dione

: 86814-89-3
10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / acetone

2: 91 percent / pyridine / 3 h / 0 deg C to r.t.

3: 76 percent / KOtBu / dimethylsulfoxide / 0.08 h / Ambient temperature

With potassium tert-butylate; In pyridine; dimethyl sulfoxide; acetone;

Reference yield:

: 75529-48-5,86814-82-6
trans-5,6-bis(hydroxymethyl)cyclohexa-1,3-diene

: 86814-89-3
10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / acetone

2: 91 percent / pyridine / 3 h / 0 deg C to r.t.

3: 76 percent / KOtBu / dimethylsulfoxide / 0.08 h / Ambient temperature

With potassium tert-butylate; In pyridine; dimethyl sulfoxide; acetone;