4,7-anhydro-1,2,3-trideoxy-1-[(diphenoxyphosphoryl)amino]-5,6,8-tri-O-methyl-D-altrooctitol

Base Information

Chemical Name:4,7-anhydro-1,2,3-trideoxy-1-[(diphenoxyphosphoryl)amino]-5,6,8-tri-O-methyl-D-altrooctitol
CAS No.:1185548-04-2
Molecular Formula:C₂₃H₃₂NO₇P
Molecular Weight:465.483
Hs Code.:

Synonyms:4,7-anhydro-1,2,3-trideoxy-1-[(diphenoxyphosphoryl)amino]-5,6,8-tri-O-methyl-D-altrooctitol

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Chemical Property of 4,7-anhydro-1,2,3-trideoxy-1-[(diphenoxyphosphoryl)amino]-5,6,8-tri-O-methyl-D-altrooctitol

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Technology Process of 4,7-anhydro-1,2,3-trideoxy-1-[(diphenoxyphosphoryl)amino]-5,6,8-tri-O-methyl-D-altrooctitol

There total 1 articles about 4,7-anhydro-1,2,3-trideoxy-1-[(diphenoxyphosphoryl)amino]-5,6,8-tri-O-methyl-D-altrooctitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1071715-94-0
(PhO)2POCl

: 1185548-02-0
4,7-anhydro-1-azido-1,2,3-trideoxy-5,6,8-tri-O-methyl-D-altrooctitol

: 1185548-04-2
4,7-anhydro-1,2,3-trideoxy-1-[(diphenoxyphosphoryl)amino]-5,6,8-tri-O-methyl-D-altrooctitol

Guidance literature:: 4,7-anhydro-1-azido-1,2,3-trideoxy-5,6,8-tri-O-methyl-D-altrooctitol; With 10% palladium on activated carbon; hydrogen; In ethyl acetate;

(PhO)2POCl; With triethylamine; In chloroform; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.05.049

Reference yield: 64.0%

: 1185548-04-2
4,7-anhydro-1,2,3-trideoxy-1-[(diphenoxyphosphoryl)amino]-5,6,8-tri-O-methyl-D-altrooctitol

: 1185548-46-2
(4S)-1,4:4,7-dianhydro-1,2,3-trideoxy-1-[(diphenoxyphosphoryl)amino]-5,6,8-tri-O-methyl-D-ribo-oct-4-ulose

Guidance literature:: With [bis(acetoxy)iodo]benzene; iodine; In dichloromethane; at 20 ℃; stereoselective reaction; Inert atmosphere; Irradiation;
DOI:10.1016/j.tet.2009.05.049