methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside
CAS No.:470665-48-6
Molecular Formula:C₃₂H₅₁NO₈
Molecular Weight:577.759
Hs Code.:

Synonyms:methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

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Chemical Property of methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

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Technology Process of methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

There total 5 articles about methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 544-63-8
n-tetradecanoic acid

: 61348-62-7
methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-α-D-glucopyranoside

: 470665-48-6
methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1081/CAR-120004331

Reference yield:

: 14131-62-5
D-glucosamine hydrochloride

: 470665-48-6
methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃ / H₂O / 16 h / 20 °C

2: 16 g / HCl / 7 h / Heating

3: 100 percent / p-toluenesulfonic acid / acetone; CH₂Cl₂ / 16 h / 20 °C

4: 86 percent / DMAP; DCC / CH₂Cl₂ / 18 h / 20 °C

With hydrogenchloride; dmap; sodium hydrogencarbonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In dichloromethane; water; acetone;
DOI:10.1081/CAR-120004331

Reference yield:

: 77059-32-6
benzyl ((2S,3R,4R,5S,6R)-2,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-3-yl)carbamate

: 470665-48-6
methyl 2-[(benzyloxycarbonyl)amino]-2-deoxy-4,6-isopropylidene-3-O-tetradecanoyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 16 g / HCl / 7 h / Heating

2: 100 percent / p-toluenesulfonic acid / acetone; CH₂Cl₂ / 16 h / 20 °C

3: 86 percent / DMAP; DCC / CH₂Cl₂ / 18 h / 20 °C

With hydrogenchloride; dmap; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In dichloromethane; acetone;
DOI:10.1081/CAR-120004331