Technology Process of C27H20N3O5S(1-)*Na(1+)
There total 5 articles about C27H20N3O5S(1-)*Na(1+) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
acetonitrile;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: copper(II) sulfate / methanol / 80 °C
2.1: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 20 °C
3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere
4.1: lithium hydroxide / tetrahydrofuran; water / 20 °C
4.2: pH 4.0
5.1: sodium hydroxide / acetonitrile / 0.5 h
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tert.-butylnitrite; sodium carbonate; copper(II) sulfate; sodium hydroxide; copper(ll) bromide; lithium hydroxide;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; acetonitrile;
3.1: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 20 °C
2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere
3.1: lithium hydroxide / tetrahydrofuran; water / 20 °C
3.2: pH 4.0
4.1: sodium hydroxide / acetonitrile / 0.5 h
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tert.-butylnitrite; sodium carbonate; sodium hydroxide; copper(ll) bromide; lithium hydroxide;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; acetonitrile;
2.1: |Suzuki Coupling;