(S_S,S)-(+)-N-(p-toluenesulfinyl)-2-(1-amino-2-methylpropyl)-2-methyl-1,3-dithiane

Base Information

• Chemical Name: (S_S,S)-(+)-N-(p-toluenesulfinyl)-2-(1-amino-2-methylpropyl)-2-methyl-1,3-dithiane
• CAS No.: 770743-74-3
• Molecular Formula: C₁₆H₂₅NOS₃
• Molecular Weight: 343.579

Synonyms:(S_S,S)-(+)-N-(p-toluenesulfinyl)-2-(1-amino-2-methylpropyl)-2-methyl-1,3-dithiane

Chemical Property of (S_S,S)-(+)-N-(p-toluenesulfinyl)-2-(1-amino-2-methylpropyl)-2-methyl-1,3-dithiane

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of (S_S,S)-(+)-N-(p-toluenesulfinyl)-2-(1-amino-2-methylpropyl)-2-methyl-1,3-dithiane

There total 1 articles about (S_S,S)-(+)-N-(p-toluenesulfinyl)-2-(1-amino-2-methylpropyl)-2-methyl-1,3-dithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-methyl-1,3-dithian (6007-26-7) + (S)-(+)-N-(isopropylmethylidene)-p-toluenesulfinamide (158009-36-0) → (SS,S)-(+)-N-(p-toluenesulfinyl)-2-(1-amino-2-methylpropyl)-2-methyl-1,3-dithiane (770743-74-3)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

DOI:10.1021/ol0485971

Reference yield: 60.0%

(SS,S)-(+)-N-(p-toluenesulfinyl)-2-(1-amino-2-methylpropyl)-2-methyl-1,3-dithiane (770743-74-3) → (SS,S)-(+)-N-(p-toluenesulfinyl)-3-amino-3-isopropyl-2-propanone

Guidance literature:

With bis-[(trifluoroacetoxy)iodo]benzene; In water; acetonitrile; at -20 ℃; for 0.333333h;

DOI:10.1021/ol0485971

upstream raw materials:

2-methyl-1,3-dithian

(S)-(+)-N-(isopropylmethylidene)-p-toluenesulfinamide

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