OsH(η5-C5H4(CH2)2PPh2)(P(i)Pr3)

Base Information

• Chemical Name: OsH(η5-C5H4(CH2)2PPh2)(P(i)Pr3)
• CAS No.: 713528-58-6
• Molecular Formula: C₂₈H₄₀OsP₂
• Molecular Weight: 628.773
• Mol file: 713528-58-6.mol

Synonyms:OsH(η5-C5H4(CH2)2PPh2)(P(i)Pr3)

Chemical Property of OsH(η5-C5H4(CH2)2PPh2)(P(i)Pr3)

Chemical Property:

Purity/Quality:

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Technology Process of OsH(η5-C5H4(CH2)2PPh2)(P(i)Pr3)

There total 1 articles about OsH(η5-C5H4(CH2)2PPh2)(P(i)Pr3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

[OsH2(η5-C5H4(CH2)2PPh2)(P(i)Pr3)]Cl (713528-57-5) → OsH(η5-C5H4(CH2)2PPh2)(P(i)Pr3) (713528-58-6)

Guidance literature:

With KOH; In tetrahydrofuran; methanol; byproducts: KCl, H2O; under Ar; soln. of KOH in MeOH added to soln. Os complex in THF, mixt. stirred at room temp. for 12 h; solvent removed in vacuo, residue extd. with pentane, filtrate concd. todryness, residue washed with cold isopropanol and dried in vacuo;

DOI:10.1021/om049904+

upstream raw materials:

[OsH2(η5-C5H4(CH2)2PPh2)(P(i)Pr3)]Cl

Refernces