methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate

Base Information

Chemical Name:methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate
CAS No.:436155-45-2
Molecular Formula:C₁₄H₁₉BrN₂O₆
Molecular Weight:391.219
Hs Code.:

Synonyms:methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate

Suppliers and Price of methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate

There total 3 articles about methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 156141-42-3
methyl 2-[3-(3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate

: 436155-45-2
methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate

Guidance literature:: methyl 2-[3-(3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate; With N-Bromosuccinimide; In dichloromethane; at 20 ℃; for 0.25h;

With trifluoroacetic acid; In dichloromethane; Further stages.;
DOI:10.1039/b110414d

Reference yield:

: 53560-25-1
methyl 3-(3,4,5-trimethoxyphenyl)propionate

: 436155-45-2
methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 85 percent / hydrazine hydrate / 110 - 120 °C

2.1: 92 percent / sodium bicarbonate / CH₂Cl₂ / 20 °C

3.1: NBS / CH₂Cl₂ / 0.25 h / 20 °C

3.2: 98 percent / TFA / CH₂Cl₂

With N-Bromosuccinimide; sodium hydrogencarbonate; hydrazine hydrate; In dichloromethane;
DOI:10.1039/b110414d

Reference yield:

: 257284-96-1
3-(3,4,5-trimethoxyphenyl)propanoylhydrazine

: 436155-45-2
methyl 2-[3-(2-bromo-3,4,5-trimethoxyphenyl)propanoyl]hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 92 percent / sodium bicarbonate / CH₂Cl₂ / 20 °C

2.1: NBS / CH₂Cl₂ / 0.25 h / 20 °C

2.2: 98 percent / TFA / CH₂Cl₂

With N-Bromosuccinimide; sodium hydrogencarbonate; In dichloromethane;
DOI:10.1039/b110414d