(Z)-3-[N'-((Z)-3-Imino-1-methyl-3-p-tolyl-propenyl)-hydrazino]-1-p-tolyl-but-2-enylideneamine

Base Information

• Chemical Name: (Z)-3-[N'-((Z)-3-Imino-1-methyl-3-p-tolyl-propenyl)-hydrazino]-1-p-tolyl-but-2-enylideneamine
• CAS No.: 105687-01-2
• Molecular Formula: C₂₂H₂₆N₄
• Molecular Weight: 346.475

Synonyms:(Z)-3-[N'-((Z)-3-Imino-1-methyl-3-p-tolyl-propenyl)-hydrazino]-1-p-tolyl-but-2-enylideneamine

Chemical Property of (Z)-3-[N'-((Z)-3-Imino-1-methyl-3-p-tolyl-propenyl)-hydrazino]-1-p-tolyl-but-2-enylideneamine

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Technology Process of (Z)-3-[N'-((Z)-3-Imino-1-methyl-3-p-tolyl-propenyl)-hydrazino]-1-p-tolyl-but-2-enylideneamine

There total 1 articles about (Z)-3-[N'-((Z)-3-Imino-1-methyl-3-p-tolyl-propenyl)-hydrazino]-1-p-tolyl-but-2-enylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

para-methylbenzonitrile (104-85-8) + propan-2-one azine (627-70-3) → (Z)-3-[N'-((Z)-3-Imino-1-methyl-3-p-tolyl-propenyl)-hydrazino]-1-p-tolyl-but-2-enylideneamine (105687-01-2)

Guidance literature:

With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) diethyl ether, 20 min, 2.) -78 deg C to room temp.;

DOI:10.1039/c39820000454

Reference yield: 93.0%

carbon disulfide (75-15-0,12122-00-8) + (Z)-3-[N'-((Z)-3-Imino-1-methyl-3-p-tolyl-propenyl)-hydrazino]-1-p-tolyl-but-2-enylideneamine (105687-01-2) → 1-(3-imino-1-methyl-3-p-tolylprop-1-enyl)-5-isothiocyanato-3-methyl-5-p-tolyl-2-pyrazoline (122851-98-3)

Guidance literature:

In tetrahydrofuran; at 80 ℃; for 20h; sealed tube;

DOI:10.1016/S0040-4020(01)80043-0

Reference yield: 78.0%

(Z)-3-[N'-((Z)-3-Imino-1-methyl-3-p-tolyl-propenyl)-hydrazino]-1-p-tolyl-but-2-enylideneamine (105687-01-2) → 2,7-Dimethyl-3a,5-di-p-tolyl-3,3a-dihydro-pyrazolo[1,5-a]pyrimidine (82737-58-4)

Guidance literature:

With sulfuric acid; Ambient temperature;

DOI:10.1039/c39820000454

upstream raw materials:

para-methylbenzonitrile

propan-2-one azine

Downstream raw materials:

1-(3-imino-1-methyl-3-p-tolylprop-1-enyl)-5-isothiocyanato-3-methyl-5-p-tolyl-2-pyrazoline

[(Z)-3-(N'-{(Z)-3-[(E)-Ethoxycarbonylimino]-1-methyl-3-p-tolyl-propenyl}-hydrazino)-1-p-tolyl-but-2-en-(E)-ylidene]-carbamic acid ethyl ester

2,7-Dimethyl-3a,5-di-p-tolyl-3,3a-dihydro-pyrazolo[1,5-a]pyrimidine

6,6'-Dimethyl-4,4'-di-p-tolyl-[1,1']bipyrimidinyl-2,2'-dione

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