acetic acid 2-{[pent-4-enyl-(toluene-4-sulfonyl)-amino]-methyl}-allyl ester

Base Information

Chemical Name:acetic acid 2-{[pent-4-enyl-(toluene-4-sulfonyl)-amino]-methyl}-allyl ester
CAS No.:935553-08-5
Molecular Formula:C₁₈H₂₅NO₄S
Molecular Weight:351.467
Hs Code.:

Synonyms:acetic acid 2-{[pent-4-enyl-(toluene-4-sulfonyl)-amino]-methyl}-allyl ester

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Chemical Property of acetic acid 2-{[pent-4-enyl-(toluene-4-sulfonyl)-amino]-methyl}-allyl ester

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Technology Process of acetic acid 2-{[pent-4-enyl-(toluene-4-sulfonyl)-amino]-methyl}-allyl ester

There total 1 articles about acetic acid 2-{[pent-4-enyl-(toluene-4-sulfonyl)-amino]-methyl}-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 130239-36-0
3-bromo-2-acetoxymethylpropene

: 81097-24-7
N-tosyl-(4-pentenyl)amine

: 935553-08-5
acetic acid 2-{[pent-4-enyl-(toluene-4-sulfonyl)-amino]-methyl}-allyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/jo0624896

Reference yield: 70.0%

: 935553-08-5
acetic acid 2-{[pent-4-enyl-(toluene-4-sulfonyl)-amino]-methyl}-allyl ester

: 935553-12-1
acetic acid 1-(toluene-4-sulfonyl)-2,5,6,7-tetrahydro-1H-azepin-3-ylmethyl ester

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 2h; Heating;
DOI:10.1021/jo0624896

Reference yield:

: 935553-08-5
acetic acid 2-{[pent-4-enyl-(toluene-4-sulfonyl)-amino]-methyl}-allyl ester

: 3-methylene-1-(toluene-4-sulfonyl)-azepane

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / second generation Grubbs' catalyst / CH₂Cl₂ / 2 h / Heating

2: 82 percent Spectr_. / triethylamine; formic acid; di-tert-butyl(2'-methylbiphenyl-2-yl)phosphine / allylpalladium chloride dimer / dimethylformamide / 18 h / 0 °C

With formic acid; triethylamine; di-tert-butyl (2'-methyl-[1,1'-biphenyl]-2-yl)phosphine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; bis(η3-allyl-μ-chloropalladium(II)); In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0624896