(2S)-2-(4-(N-Boc-N-2-picolyl aminomethyl) benzoyl)-5-(pyridin-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

Base Information

Chemical Name:(2S)-2-(4-(N-Boc-N-2-picolyl aminomethyl) benzoyl)-5-(pyridin-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide
CAS No.:477558-56-8
Molecular Formula:C₄₁H₄₆N₆O₄
Molecular Weight:686.854
Hs Code.:

Synonyms:(2S)-2-(4-(N-Boc-N-2-picolyl aminomethyl) benzoyl)-5-(pyridin-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

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Chemical Property of (2S)-2-(4-(N-Boc-N-2-picolyl aminomethyl) benzoyl)-5-(pyridin-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

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Technology Process of (2S)-2-(4-(N-Boc-N-2-picolyl aminomethyl) benzoyl)-5-(pyridin-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

There total 1 articles about (2S)-2-(4-(N-Boc-N-2-picolyl aminomethyl) benzoyl)-5-(pyridin-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 504-29-0
2-aminopyridine

: 369656-62-2
N-[(1S)-1-(1-naphthyl)ethyl]-5-hydroxy-2-(S)-[4-[N-Boc-N-(pyridin-2-ylmethyl)aminomethyl]benzoylamino]pentanoylamide

: 477558-56-8
(2S)-2-(4-(N-Boc-N-2-picolyl aminomethyl) benzoyl)-5-(pyridin-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

Guidance literature:: N-[(1S)-1-(1-naphthyl)ethyl]-5-hydroxy-2-(S)-[4-[N-Boc-N-(pyridin-2-ylmethyl)aminomethyl]benzoylamino]pentanoylamide; With N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; In chloroform; water; at 20 ℃; for 5h;

2-aminopyridine; With triethylamine; In methanol; pH=9; Molecular sieve;

With sodium cyanoborohydride; acetic acid; In methanol; pH=4;

Reference yield:

: 477558-56-8
(2S)-2-(4-(N-Boc-N-2-picolyl aminomethyl) benzoyl)-5-(pyridin-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide

: (2S)-2-(4-(2-picolyl)aminomethyl)benzoyl-5-(pyridin-2-yl)aminovalerate (1'S)-1'-(1-naphthyl) ethylamide hydrochloride

Guidance literature:: (2S)-2-(4-(N-Boc-N-2-picolyl aminomethyl) benzoyl)-5-(pyridin-2-yl) aminovalerate (1'S)-1'-(1-naphthyl) ethylamide; With hydrogenchloride; In 1,4-dioxane; methanol; at 20 ℃; for 2h;

With hydrogenchloride; In water;