(S)-N-(1-(4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide

Base Information

• Chemical Name: (S)-N-(1-(4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide
• CAS No.: 1028184-23-7
• Molecular Formula: C₂₂H₁₆ClF₄NO₅S₂
• Molecular Weight: 555.885

Synonyms:(S)-N-(1-(4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide

Chemical Property of (S)-N-(1-(4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide

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Technology Process of (S)-N-(1-(4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide

There total 4 articles about (S)-N-(1-(4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(1-{4-(4-chloro-2-(2-fluoro(13C)phenylsulfanyl)benzenesulfonyl)phenyl}ethyl)-2,2,2-trifluoroacetamide (1028184-21-5) → (S)-N-(1-(4-((4-chloro-2-((2-fluoro(13C6)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide (1028184-23-7)

Guidance literature:

With dihydrogen peroxide; urea; trifluoroacetic anhydride; In ethyl acetate; acetonitrile; at 20 ℃; for 2.5h;

DOI:10.1002/jlcr.1183

Reference yield:

N-{1-[4-(4-chlorobenzenesulfonyl)-phenyl]ethyl}-2,2,2-trifluoroacetamide (447460-00-6) → (S)-N-(1-(4-((4-chloro-2-((2-fluoro(13C6)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide (1028184-23-7)

Guidance literature:

Multi-step reaction with 2 steps

1: urea; hydrogen peroxide; trifluoroacetic anhydride / acetonitrile; ethyl acetate / 2.5 h / 20 °C

With dihydrogen peroxide; urea; trifluoroacetic anhydride; In ethyl acetate; acetonitrile;

DOI:10.1002/jlcr.1183

Reference yield:

C3(13)C6H9FOS2 (1028184-51-1) → (S)-N-(1-(4-((4-chloro-2-((2-fluoro(13C6)phenyl)sulfoxyl)phenyl)sulfonyl)phenyl)-ethyl)-2,2,2-trifluoroacetamide (1028184-23-7)

Guidance literature:

Multi-step reaction with 2 steps

1: urea; hydrogen peroxide; trifluoroacetic anhydride / acetonitrile; ethyl acetate / 2.5 h / 20 °C

With dihydrogen peroxide; urea; trifluoroacetic anhydride; In ethyl acetate; acetonitrile;

DOI:10.1002/jlcr.1183

upstream raw materials:

N-{1-[4-(4-chlorobenzenesulfonyl)-phenyl]ethyl}-2,2,2-trifluoroacetamide

C₃⁽¹³⁾C₆H₉FOS₂

N-(1-{4-(4-chloro-2-(2-fluoro(¹³C)phenylsulfanyl)benzenesulfonyl)phenyl}ethyl)-2,2,2-trifluoroacetamide

Downstream raw materials:

(S)-4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)sulfonyl)phenyl)sulfonyl)-alpha-methylbenzenemethanamine

(S)-N-(1-(4-((4-chloro-2-((2-fluoro(¹³C₆)phenyl)-sulfonyl)phenyl)sulfonyl)phenyl)-ethyl)trifluoromethanesulfonamide

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