Technology Process of C23H24N6O4S
There total 7 articles about C23H24N6O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C23H25N3O5S;
With
sodium azide; zinc dibromide;
In
water;
at 105 ℃;
for 72h;
Heating / reflux;
With
hydrogenchloride;
In
water; ethyl acetate;
for 0.5h;
pH=1;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C
2.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 - 70 °C
3.1: sodium azide; zinc dibromide / water / 72 h / 105 °C / Heating / reflux
3.2: 0.5 h / pH 1
With
sodium hydroxide; sodium azide; 1-hydroxy-7-aza-benzotriazole; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; zinc dibromide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hydroxide; water / tetrahydrofuran / 12 h / 45 °C
1.2: pH 2
2.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C
3.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 - 70 °C
4.1: sodium azide; zinc dibromide / water / 72 h / 105 °C / Heating / reflux
4.2: 0.5 h / pH 1
With
lithium hydroxide; sodium hydroxide; sodium azide; 1-hydroxy-7-aza-benzotriazole; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; zinc dibromide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;