C₁₈H₂₀O

Base Information

Chemical Name:C₁₈H₂₀O
CAS No.:1350626-76-4
Molecular Formula:C₁₈H₂₀O
Molecular Weight:252.356
Hs Code.:

Synonyms:C₁₈H₂₀O

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Chemical Property of C₁₈H₂₀O

Chemical Property:

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Technology Process of C₁₈H₂₀O

There total 6 articles about C₁₈H₂₀O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 591-50-4
iodobenzene

: 1350626-75-3
C₁₈H₃₀O₂Si

: 1350626-76-4
C₁₈H₂₀O

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ja209553f

Reference yield:

: 1172850-67-7
C₁₇H₂₂O₂

: 1350626-76-4
C₁₈H₂₀O

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C / Inert atmosphere

2: 1H-imidazole / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

3: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / 5,5-dimethyl-1,3-cyclohexadiene / 3 h / 80 °C / Inert atmosphere

4: water; potassium carbonate / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / 4 h / 20 °C / Inert atmosphere

5: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

With 1H-imidazole; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; tetrabutyl ammonium fluoride; water; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; 5: Hiyama coupling;
DOI:10.1021/ja209553f

Reference yield:

: C₂₂H₃₇ClOSi₂

: 1350626-76-4
C₁₈H₂₀O

Guidance literature:: Multi-step reaction with 2 steps

1: water; potassium carbonate / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / 4 h / 20 °C / Inert atmosphere

2: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tetrabutyl ammonium fluoride; water; potassium carbonate; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; 2: Hiyama coupling;
DOI:10.1021/ja209553f