{2-[2,3-Bis-(2-dimethylaminomethyl-phenyl)-1,2,3-tris-(2,4,6-trimethyl-phenyl)-trisiliran-1-yl]-benzyl}-dimethyl-amine

Base Information

• Chemical Name: {2-[2,3-Bis-(2-dimethylaminomethyl-phenyl)-1,2,3-tris-(2,4,6-trimethyl-phenyl)-trisiliran-1-yl]-benzyl}-dimethyl-amine
• CAS No.: 210547-70-9
• Molecular Formula: C₅₄H₆₉N₃Si₃
• Molecular Weight: 844.418

Synonyms:{2-[2,3-Bis-(2-dimethylaminomethyl-phenyl)-1,2,3-tris-(2,4,6-trimethyl-phenyl)-trisiliran-1-yl]-benzyl}-dimethyl-amine

Chemical Property of {2-[2,3-Bis-(2-dimethylaminomethyl-phenyl)-1,2,3-tris-(2,4,6-trimethyl-phenyl)-trisiliran-1-yl]-benzyl}-dimethyl-amine

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Technology Process of {2-[2,3-Bis-(2-dimethylaminomethyl-phenyl)-1,2,3-tris-(2,4,6-trimethyl-phenyl)-trisiliran-1-yl]-benzyl}-dimethyl-amine

There total 3 articles about {2-[2,3-Bis-(2-dimethylaminomethyl-phenyl)-1,2,3-tris-(2,4,6-trimethyl-phenyl)-trisiliran-1-yl]-benzyl}-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-(dimethylaminomethyl)phenyl-(2,4,6-trimethylphenyl)silane (210547-62-9) → {2-[2,3-Bis-(2-dimethylaminomethyl-phenyl)-1,2,3-tris-(2,4,6-trimethyl-phenyl)-trisiliran-1-yl]-benzyl}-dimethyl-amine (210547-70-9)

Guidance literature:

With magnesium; In tetrahydrofuran; for 168h; Ambient temperature;

DOI:10.1002/(SICI)1521-3765(19980515)4:5<852::AID-CHEM852>3.0.CO;2-7

Reference yield:

2,4,6-trimethyl-phenyl-trichlorosilane (17902-75-9) → {2-[2,3-Bis-(2-dimethylaminomethyl-phenyl)-1,2,3-tris-(2,4,6-trimethyl-phenyl)-trisiliran-1-yl]-benzyl}-dimethyl-amine (210547-70-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / diethyl ether / 16 h / Ambient temperature

2: 65 percent / Mg / tetrahydrofuran / 168 h / Ambient temperature

With magnesium; In tetrahydrofuran; diethyl ether;

DOI:10.1002/(SICI)1521-3765(19980515)4:5<852::AID-CHEM852>3.0.CO;2-7

Reference yield:

2-(N,N-dimethylaminomethyl)phenyllithium (56174-66-4) → {2-[2,3-Bis-(2-dimethylaminomethyl-phenyl)-1,2,3-tris-(2,4,6-trimethyl-phenyl)-trisiliran-1-yl]-benzyl}-dimethyl-amine (210547-70-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / diethyl ether / 16 h / Ambient temperature

2: 65 percent / Mg / tetrahydrofuran / 168 h / Ambient temperature

With magnesium; In tetrahydrofuran; diethyl ether;

DOI:10.1002/(SICI)1521-3765(19980515)4:5<852::AID-CHEM852>3.0.CO;2-7

upstream raw materials:

2-(dimethylaminomethyl)phenyl-(2,4,6-trimethylphenyl)silane

2,4,6-trimethyl-phenyl-trichlorosilane

2-(N,N-dimethylaminomethyl)phenyllithium

Downstream raw materials:

{2-[1,2-Dichloro-2-(2-dimethylaminomethyl-phenyl)-1,2-bis-(2,4,6-trimethyl-phenyl)-disilanyl]-benzyl}-dimethyl-amine

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