(2R,3R,4R)-3-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-2-hydroxyhex-5-enyl benzoate

Base Information

Chemical Name:(2R,3R,4R)-3-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-2-hydroxyhex-5-enyl benzoate
CAS No.:1219744-60-1
Molecular Formula:C₂₂H₃₂O₆Si
Molecular Weight:420.578
Hs Code.:

Synonyms:(2R,3R,4R)-3-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-2-hydroxyhex-5-enyl benzoate

Suppliers and Price of (2R,3R,4R)-3-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-2-hydroxyhex-5-enyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4R)-3-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-2-hydroxyhex-5-enyl benzoate

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Technology Process of (2R,3R,4R)-3-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-2-hydroxyhex-5-enyl benzoate

There total 1 articles about (2R,3R,4R)-3-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-2-hydroxyhex-5-enyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1219744-59-8
C₁₅H₂₆O₄Si

: 65-85-0,8013-63-6
benzoic acid

: 1219744-60-1
(2R,3R,4R)-3-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-2-hydroxyhex-5-enyl benzoate

: 1219744-62-3
(2R,3R,4R)-2-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-3-hydroxyhex-5-enyl benzoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 20 ℃; for 46h;
DOI:10.1021/jo1002642

Reference yield: 75.0%

: 1219744-60-1
(2R,3R,4R)-3-(acryloyloxy)-4-(tert-butyldimethylsilyloxy)-2-hydroxyhex-5-enyl benzoate

: 1219744-61-2
(R)-2-((2R,3R)-3-(tert-butyldimethylsilyloxy)-6-oxo-3,6-dihydro-2H-pyran-2-yl)-2-hydroxyethyl benzoate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; phenol; In toluene; at 70 ℃; for 6h; Inert atmosphere;
DOI:10.1021/jo1002642