Technology Process of C14H16O3
There total 4 articles about C14H16O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
toluene;
for 2h;
Inert atmosphere;
Reflux;
DOI:10.1021/ol300494q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: quinoline; rosenmund catalyst; hydrogen / ethyl acetate
3.1: toluene-4-sulfonic acid / toluene / 2 h / Inert atmosphere; Reflux
With
quinoline; n-butyllithium; rosenmund catalyst; hydrogen; toluene-4-sulfonic acid;
In
tetrahydrofuran; ethyl acetate; toluene;
DOI:10.1021/ol300494q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: quinoline; rosenmund catalyst; hydrogen / ethyl acetate
3.1: toluene-4-sulfonic acid / toluene / 2 h / Inert atmosphere; Reflux
With
quinoline; n-butyllithium; rosenmund catalyst; hydrogen; toluene-4-sulfonic acid;
In
tetrahydrofuran; ethyl acetate; toluene;
DOI:10.1021/ol300494q