(N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol)

Base Information

Chemical Name:(N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol)
CAS No.:688365-40-4
Molecular Formula:C₃₆H₄₇N₃O₇
Molecular Weight:633.785
Hs Code.:

Synonyms:(N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol)

Suppliers and Price of (N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol)

Chemical Property:

Purity/Quality:

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Technology Process of (N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol)

There total 1 articles about (N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 688365-39-1
C₃₅H₄₅N₃O₇

: 18107-18-1
diazomethyl-trimethyl-silane

: 688365-40-4
(N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol)

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In methanol; chloroform; at 20 ℃; for 72h;
DOI:10.1271/bbb.69.1733

Reference yield:

: 688365-40-4
(N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol)

: 688365-41-5
C₂₉H₄₁N₃O₇

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 18h;
DOI:10.1271/bbb.69.1733

Reference yield:

: 688365-40-4
(N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(4'-O-methyl-L-tyrosinol)

: 688365-44-8
C₃₆H₄₁N₃O₆

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / Pd/C / methanol / 18 h / 20 °C

2: pyridine / 18 h / 20 °C

3: trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

4: water-soluble carbodiimide hydrochloride; 1-hydroxybenzotriazole; triethylamine / dimethylformamide / 18 h / 20 °C

5: K₂CO₃ / methanol / 18 h / 20 °C

With pyridine; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1271/bbb.69.1733