dimethoxy-3,5-1 benzene

Base Information

• Chemical Name: dimethoxy-3,5-1 benzene
• CAS No.: 85604-63-3
• Molecular Formula: C₁₃H₁₈O₄
• Molecular Weight: 238.284

Synonyms:dimethoxy-3,5-1 benzene

Chemical Property of dimethoxy-3,5-1 benzene

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Technology Process of dimethoxy-3,5-1 benzene

There total 2 articles about dimethoxy-3,5-1 benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3,4-dihydro-2H-pyran (110-87-2) + 3,5-dimethoxyphenol (500-99-2) → dimethoxy-3,5-1 benzene (85604-63-3)

Guidance literature:

With dimethylbromosulphonium bromide; at 20 ℃; for 0.333333h;

DOI:10.1002/ejoc.200300429

Reference yield: 36.0%

3,4-dihydro-2H-pyran (110-87-2) + 3,5-dimethoxyphenol (500-99-2) → dimethoxy-3,5-1 benzene (85604-63-3) + dimethoxy-3,5-2 phenol (118971-70-3)

Guidance literature:

With pyridinium p-toluenesulfonate; In dichloromethane; for 20h; Ambient temperature;

upstream raw materials:

3,4-dihydro-2H-pyran

3,5-dimethoxyphenol

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