μ-{(porphyrazine-2,3,7,8,12,13,17,18-octathiolato)copper(II)-(S,N,S)4}tetrakis(di-tert-butyltin(IV))*benzene

Base Information

Chemical Name:μ-{(porphyrazine-2,3,7,8,12,13,17,18-octathiolato)copper(II)-(S,N,S)4}tetrakis(di-tert-butyltin(IV))*benzene
CAS No.:141272-50-6
Molecular Formula:C₆H₆*C₄₈H₇₂CuN₈S₈Sn₄
Molecular Weight:1634.18
Hs Code.:

Synonyms:μ-{(porphyrazine-2,3,7,8,12,13,17,18-octathiolato)copper(II)-(S,N,S)4}tetrakis(di-tert-butyltin(IV))*benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of μ-{(porphyrazine-2,3,7,8,12,13,17,18-octathiolato)copper(II)-(S,N,S)4}tetrakis(di-tert-butyltin(IV))*benzene

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Technology Process of μ-{(porphyrazine-2,3,7,8,12,13,17,18-octathiolato)copper(II)-(S,N,S)4}tetrakis(di-tert-butyltin(IV))*benzene

There total 1 articles about μ-{(porphyrazine-2,3,7,8,12,13,17,18-octathiolato)copper(II)-(S,N,S)4}tetrakis(di-tert-butyltin(IV))*benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 141272-49-3
{2,3,7,8,12,13,17,18-octakis(benzylthio)porphyrazinato}copper(II)

: 141272-51-7
di-tert-butyltin(IV) dinitrate

: 141272-50-6
μ-{(porphyrazine-2,3,7,8,12,13,17,18-octathiolato)copper(II)-(S,N,S)4}tetrakis(di-tert-butyltin(IV))*benzene

Guidance literature:: With Na; NH₃; NH₄NO₃; In tetrahydrofuran; suspending the Cu complex in liquid NH3 and THF at -78°C, addn. of Na, reflux at -33°C for 30 min., slow (!) addn. of NH4NO3, removing of THF in vac., addn. of the Sn nitrate, 30 min. stirring; filtn., washing of solid with MeOH, soluting in hot benzene, drying, elem. anal.;
DOI:10.1021/ja00045a013