2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate

Base Information

Chemical Name:2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate
CAS No.:1258410-92-2
Molecular Formula:C₄₂H₃₅NO₁₀S
Molecular Weight:745.807
Hs Code.:

Synonyms:2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate

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Chemical Property of 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate

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Technology Process of 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate

There total 4 articles about 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1258410-91-1
2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate

: 1258410-92-2
2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 1 h / 20 °C / pH 9

2: pyridine / 0 - 20 °C / Inert atmosphere

With pyridine; sodium methylate; In methanol;
DOI:10.1021/ol1023079

Reference yield:

: 13509-41-6
methyl N-phenylthiocarbamate

: 1258410-92-2
2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / acetonitrile / 1 h / 20 °C

2: sodium methylate / methanol / 1 h / 20 °C / pH 9

3: pyridine / 0 - 20 °C / Inert atmosphere

With pyridine; sodium methylate; sodium hydroxide; In methanol; acetonitrile;
DOI:10.1021/ol1023079

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 1258410-92-2
2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranosyl O-methyl phenylcarbamothioate

Guidance literature:: Multi-step reaction with 4 steps

1: 0.25 h / 20 °C

2: sodium hydroxide / acetonitrile / 1 h / 20 °C

3: sodium methylate / methanol / 1 h / 20 °C / pH 9

4: pyridine / 0 - 20 °C / Inert atmosphere

With pyridine; sodium methylate; sodium hydroxide; In methanol; acetonitrile;
DOI:10.1021/ol1023079