(E)-4,8-ditert-butyl-6-(2,4,6-trimethylstyryl)-2,10-dimethyl-12H-dibenzo[d,g][1,3,2]dioxaborocine

Base Information

Chemical Name:(E)-4,8-ditert-butyl-6-(2,4,6-trimethylstyryl)-2,10-dimethyl-12H-dibenzo[d,g][1,3,2]dioxaborocine
CAS No.:1266658-25-6
Molecular Formula:C₃₄H₄₃BO₂
Molecular Weight:494.525
Hs Code.:

Synonyms:(E)-4,8-ditert-butyl-6-(2,4,6-trimethylstyryl)-2,10-dimethyl-12H-dibenzo[d,g][1,3,2]dioxaborocine

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Chemical Property of (E)-4,8-ditert-butyl-6-(2,4,6-trimethylstyryl)-2,10-dimethyl-12H-dibenzo[d,g][1,3,2]dioxaborocine

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Technology Process of (E)-4,8-ditert-butyl-6-(2,4,6-trimethylstyryl)-2,10-dimethyl-12H-dibenzo[d,g][1,3,2]dioxaborocine

There total 2 articles about (E)-4,8-ditert-butyl-6-(2,4,6-trimethylstyryl)-2,10-dimethyl-12H-dibenzo[d,g][1,3,2]dioxaborocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 188707-76-8
4,8-di-tert-butyl-2,10-dimethyl-12H-dibenzo[d,g][1,3,2]dioxaborocine

: 769-25-5
2,4,6-trimethylstyrene

: 1266658-25-6
(E)-4,8-ditert-butyl-6-(2,4,6-trimethylstyryl)-2,10-dimethyl-12H-dibenzo[d,g][1,3,2]dioxaborocine

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; In toluene; for 18h;
DOI:10.1016/j.ica.2010.09.051

Reference yield:

: 119-47-1
2,2'-dihydroxy-5,5'-dimethyl-3,3'-di-tert-burtyl-1,1'-diphenylmethane

: 1266658-25-6
(E)-4,8-ditert-butyl-6-(2,4,6-trimethylstyryl)-2,10-dimethyl-12H-dibenzo[d,g][1,3,2]dioxaborocine

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfide borane complex / toluene / 18 h / Reflux

2: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] / toluene / 18 h

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; dimethylsulfide borane complex; In toluene;
DOI:10.1016/j.ica.2010.09.051