1,3-bis[ω-(2-hydroxymethylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine

Base Information

Chemical Name:1,3-bis[ω-(2-hydroxymethylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine
CAS No.:304022-19-3
Molecular Formula:C₂₇H₃₄N₂O₆
Molecular Weight:482.577
Hs Code.:

Synonyms:1,3-bis[ω-(2-hydroxymethylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine

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Chemical Property of 1,3-bis[ω-(2-hydroxymethylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine

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Technology Process of 1,3-bis[ω-(2-hydroxymethylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine

There total 3 articles about 1,3-bis[ω-(2-hydroxymethylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 304022-14-8
1,3-bis[ω-(2-formylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine

: 304022-19-3
1,3-bis[ω-(2-hydroxymethylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine

Guidance literature:: 1,3-bis[ω-(2-formylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine; With sodium tetrahydroborate; In methanol; at 60 ℃; for 3h;

With water; In 1,2-dichloro-ethane;

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 304022-19-3
1,3-bis[ω-(2-hydroxymethylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: MeONa / methanol / 0.17 h / 20 °C

1.2: 83 percent / dimethylformamide / 12 h / 90 - 95 °C

2.1: NaBH₄ / methanol / 3 h / 60 °C

2.2: 82 percent / water / 1,2-dichloro-ethane

With sodium tetrahydroborate; sodium methylate; In methanol; 1.1: Metallation / 1.2: Substitution / 2.1: Reduction / 2.2: Hydrolysis;

Reference yield:

: 60316-18-9
1,3-bis(ω-bromobutyl)-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine

: 304022-19-3
1,3-bis[ω-(2-hydroxymethylphenoxy)butyl]-6-methyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: MeONa / methanol / 0.17 h / 20 °C

1.2: 83 percent / dimethylformamide / 12 h / 90 - 95 °C

2.1: NaBH₄ / methanol / 3 h / 60 °C

2.2: 82 percent / water / 1,2-dichloro-ethane

With sodium tetrahydroborate; sodium methylate; In methanol; 1.1: Metallation / 1.2: Substitution / 2.1: Reduction / 2.2: Hydrolysis;