Technology Process of C36H35N3O6S2
There total 11 articles about C36H35N3O6S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
for 4h;
Inert atmosphere;
DOI:10.1002/chem.201304064
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid; sodium iodide / Reflux
2.1: tetrakis(triphenylphosphine) palladium(0); cesium fluoride / 1,4-dioxane / 3 h / Inert atmosphere; Reflux
3.1: lithium iodide / ethyl acetate / Reflux
4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / Inert atmosphere
4.2: 20 °C / Inert atmosphere
5.1: trifluoroacetic acid / dichloromethane / 4 h / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; cesium fluoride; trifluoroacetic acid; sodium iodide; lithium iodide;
In
1,4-dioxane; dichloromethane; ethyl acetate;
2.1: |Suzuki Coupling;
DOI:10.1002/chem.201304064
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: acetic acid; N-Bromosuccinimide / 2 h
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: tetrakis(triphenylphosphine) palladium(0); cesium fluoride / 1,4-dioxane / 3 h / Inert atmosphere; Reflux
4.1: lithium iodide / ethyl acetate / Reflux
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / Inert atmosphere
5.2: 20 °C / Inert atmosphere
6.1: trifluoroacetic acid / dichloromethane / 4 h / Inert atmosphere
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; cesium fluoride; trifluoroacetic acid; lithium iodide;
In
tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; ethyl acetate;
3.1: |Suzuki Coupling;
DOI:10.1002/chem.201304064