3-formyl-2,4,6-trimethylbenzenesulfonyl chloride

Base Information

• Chemical Name: 3-formyl-2,4,6-trimethylbenzenesulfonyl chloride
• CAS No.: 1403672-32-1
• Molecular Formula: C₁₀H₁₁ClO₃S
• Molecular Weight: 246.715
• Mol file: 1403672-32-1.mol

Synonyms:3-formyl-2,4,6-trimethylbenzenesulfonyl chloride

Chemical Property of 3-formyl-2,4,6-trimethylbenzenesulfonyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-formyl-2,4,6-trimethylbenzenesulfonyl chloride

There total 1 articles about 3-formyl-2,4,6-trimethylbenzenesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Potassium 3-formyl-2,4,6-trimethylbenzenesulphonate (1403672-37-6) → 3-formyl-2,4,6-trimethylbenzenesulfonyl chloride (1403672-32-1)

Guidance literature:

With 1,3,5-trichloro-2,4,6-triazine; 18-crown-6 ether; In acetone; at 50 ℃; for 48h;

DOI:10.1002/chem.201103450

Reference yield: 87.0%

3-formyl-2,4,6-trimethylbenzenesulfonyl chloride (1403672-32-1) → 3-Formyl-2,4,6-trimethylbenzenesulfonyl fluoride (139650-07-0)

Guidance literature:

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 - 50 ℃; for 29h;

DOI:10.1002/chem.201103450

Reference yield:

3-formyl-2,4,6-trimethylbenzenesulfonyl chloride (1403672-32-1) → 3-formyl-2,4,6-trimethylbenzenesulfonyl [(18)F]-fluoride (1403672-39-8)

Guidance literature:

3-formyl-2,4,6-trimethylbenzenesulfonyl chloride; With [¹⁸F]caesium fluoride; caesium carbonate; In water; tert-butyl alcohol; for 0.25h;

With pyridine; In water; tert-butyl alcohol; for 0.5h;

DOI:10.1002/chem.201103450

upstream raw materials:

Potassium 3-formyl-2,4,6-trimethylbenzenesulphonate

Downstream raw materials:

3-formyl-2,4,6-trimethylbenzenesulfonyl [⁽¹⁸⁾F]-fluoride

3-Formyl-2,4,6-trimethylbenzenesulfonyl fluoride