7-(3,5-difluoro-benzenesulfonyl)-1,2,3,4-tetrahydro-benzo[4,5]furo[2,3-c]pyridine hydrochloride

Base Information

Chemical Name:7-(3,5-difluoro-benzenesulfonyl)-1,2,3,4-tetrahydro-benzo[4,5]furo[2,3-c]pyridine hydrochloride
CAS No.:1315677-90-7
Molecular Formula:C₁₇H₁₃F₂NO₃S*ClH
Molecular Weight:385.819
Hs Code.:

Synonyms:7-(3,5-difluoro-benzenesulfonyl)-1,2,3,4-tetrahydro-benzo[4,5]furo[2,3-c]pyridine hydrochloride

Suppliers and Price of 7-(3,5-difluoro-benzenesulfonyl)-1,2,3,4-tetrahydro-benzo[4,5]furo[2,3-c]pyridine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-(3,5-difluoro-benzenesulfonyl)-1,2,3,4-tetrahydro-benzo[4,5]furo[2,3-c]pyridine hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-(3,5-difluoro-benzenesulfonyl)-1,2,3,4-tetrahydro-benzo[4,5]furo[2,3-c]pyridine hydrochloride

There total 2 articles about 7-(3,5-difluoro-benzenesulfonyl)-1,2,3,4-tetrahydro-benzo[4,5]furo[2,3-c]pyridine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1315689-49-6
7-(3,5-difluoro-phenylsulfanyl)-3,4-dihydro-1H-benzo[4,5]furo[2,3-c]pyridine-2-carboxylic acid tert-butyl ester

: 1315677-90-7
7-(3,5-difluoro-benzenesulfonyl)-1,2,3,4-tetrahydro-benzo[4,5]furo[2,3-c]pyridine hydrochloride

Guidance literature:: 7-(3,5-difluoro-phenylsulfanyl)-3,4-dihydro-1H-benzo[4,5]furo[2,3-c]pyridine-2-carboxylic acid tert-butyl ester; With 3-chloro-benzenecarboperoxoic acid; In 1,2-dichloro-ethane; for 0.166667h;

With trifluoroacetic acid; In dichloromethane; for 0.5h;

With hydrogenchloride; In diethyl ether;

Reference yield:

: 1315688-30-2
7-iodo-3,4-dihydro-1H-benzo[4,5]furo[2,3-c]pyridine-2-carboxylic acid tert-butyl ester

: 99389-26-1
3,5-difluorobenzenethiol

: 1315677-90-7
7-(3,5-difluoro-benzenesulfonyl)-1,2,3,4-tetrahydro-benzo[4,5]furo[2,3-c]pyridine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium t-butanolate / copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline / N,N-dimethyl-formamide / 16 h / 100 °C / Degassed solution

2.1: 3-chloro-benzenecarboperoxoic acid / 1,2-dichloro-ethane / 0.17 h

2.2: 0.5 h

With 3-chloro-benzenecarboperoxoic acid; sodium t-butanolate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;