(+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid

Base Information

Chemical Name:(+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid
CAS No.:123277-20-3
Molecular Formula:C₂₃H₂₄O₉
Molecular Weight:444.438
Hs Code.:

Synonyms:(+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid

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Chemical Property of (+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid

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Technology Process of (+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid

There total 1 articles about (+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 123251-30-9
(+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid lactone

: 123277-20-3
(+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid

Guidance literature:: With potassium hydroxide; In methanol; at 50 ℃; for 5h;

Reference yield: 40.0%

: 123277-20-3
(+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid

: 123251-32-1
(5R,6R,7R)-7-Hydroxymethyl-4-methoxy-5-(3,4,5-trimethoxy-phenyl)-5,6,7,8-tetrahydro-naphtho[2,3-d][1,3]dioxole-6-carboxylic acid

: 84294-81-5,94425-97-5,123287-65-0,123287-66-1
(+/-)-isopicrohernandin

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 45 ℃; for 24h; under 3420 Torr;

Reference yield:

: 123277-20-3
(+/-)-2-hydroxymethyl-5-methoxy-6,7-methylenedioxy-4-(3',4',5'-trimethoxyphenyl)-1,2-dihydro-3-naphthoic acid

: 84294-81-5,94425-97-5,123287-65-0,123287-66-1
(±)-hermandin

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / H₂ / 10percent Pd/C / ethanol / 24 h / 45 °C / 3420 Torr

2: 15 percent / DCC / CHCl₃ / 5 h / Ambient temperature

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; chloroform;