(S)-(1-(bis(dimethylamino)phosphoryl)pyrrolidin-2-yl)methyl diphenylphosphinate

Base Information

Chemical Name:(S)-(1-(bis(dimethylamino)phosphoryl)pyrrolidin-2-yl)methyl diphenylphosphinate
CAS No.:1397283-01-0
Molecular Formula:C₂₁H₃₁N₃O₃P₂
Molecular Weight:435.443
Hs Code.:

Synonyms:(S)-(1-(bis(dimethylamino)phosphoryl)pyrrolidin-2-yl)methyl diphenylphosphinate

Suppliers and Price of (S)-(1-(bis(dimethylamino)phosphoryl)pyrrolidin-2-yl)methyl diphenylphosphinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-(1-(bis(dimethylamino)phosphoryl)pyrrolidin-2-yl)methyl diphenylphosphinate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-(1-(bis(dimethylamino)phosphoryl)pyrrolidin-2-yl)methyl diphenylphosphinate

There total 1 articles about (S)-(1-(bis(dimethylamino)phosphoryl)pyrrolidin-2-yl)methyl diphenylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 16652-71-4
benzyl (2S)-2-pyrrolidinecarboxylate hydrochloride

: 1605-65-8
N,N,N',N'-Tetramethylphosphorodiamidic chloride

: 1499-21-4
Diphenylphosphinic chloride

: 1397283-01-0
(S)-(1-(bis(dimethylamino)phosphoryl)pyrrolidin-2-yl)methyl diphenylphosphinate

Guidance literature:: benzyl (2S)-2-pyrrolidinecarboxylate hydrochloride; N,N,N',N'-Tetramethylphosphorodiamidic chloride; With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Reflux;

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 5.16667h; Inert atmosphere;

Diphenylphosphinic chloride; With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.07.062