1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine

Base Information

Chemical Name:1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine
CAS No.:1316843-64-7
Molecular Formula:C₅₆H₆₃NO₁₀
Molecular Weight:910.117
Hs Code.:

1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine

Synonyms:1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine

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Chemical Property of 1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine

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Technology Process of 1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine

There total 3 articles about 1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 83051-88-1
methyl 6-aldehydo-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 674302-89-7
methyl 6-amino-2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranoside

: 1316843-64-7
1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine

Guidance literature:: methyl 6-aldehydo-2,3,4-tri-O-benzyl-α-D-glucopyranoside; methyl 6-amino-2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranoside; With titanium(IV) isopropylate; In methanol; at 0 ℃; for 3h; Inert atmosphere;

With sodium cyanoborohydride; In methanol; Inert atmosphere;
DOI:10.1002/chem.201601398

Reference yield: 48.0%

: 72471-11-5
methyl 6-deoxy-6-amino-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 34212-64-1,641635-63-4
methyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 1316843-64-7
1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; caesium carbonate; In toluene; at 120 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c1cc12800k

Reference yield: 47.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 674302-89-7
methyl 6-amino-2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranoside

: 1316843-64-7
1-((2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)-N-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)methanamine

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; caesium carbonate; In toluene; at 120 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c1cc12800k