2,2:5,5-bis(ethylenedioxy)-8-octanol

Base Information

Chemical Name:2,2:5,5-bis(ethylenedioxy)-8-octanol
CAS No.:132381-59-0
Molecular Formula:C₁₂H₂₂O₅
Molecular Weight:246.304
Hs Code.:

Synonyms:2,2:5,5-bis(ethylenedioxy)-8-octanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2:5,5-bis(ethylenedioxy)-8-octanol

Chemical Property:

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Technology Process of 2,2:5,5-bis(ethylenedioxy)-8-octanol

There total 1 articles about 2,2:5,5-bis(ethylenedioxy)-8-octanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18545-25-0
5-methyl-tetrahydro-furan-2-ol

: 132381-59-0
2,2:5,5-bis(ethylenedioxy)-8-octanol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) magnesium / 1) Et₂O; 2) Et₂O

2: 77 percent / Jones reagent / acetone / 0 °C

3: 91 percent / p-toluenesulfonic acid monohydrate / benzene

4: 1) ozone; 2) sodium borohydride / 1) MeOH, -78 deg C; 2) MeOH

With sodium tetrahydroborate; jones reagent; toluene-4-sulfonic acid; ozone; magnesium; In acetone; benzene;
DOI:10.1246/bcsj.63.3560

Reference yield:

: 132381-59-0
2,2:5,5-bis(ethylenedioxy)-8-octanol

: 4868-21-7
undec-8c-ene-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / PCC / CH₂Cl₂ / 4 h / Ambient temperature

2: 80 percent / toluene / 8 h / Ambient temperature

3: 96 percent / aq. HCl / 2 h / 50 °C

With hydrogenchloride; pyridinium chlorochromate; In dichloromethane; toluene;

Reference yield:

: 132381-59-0
2,2:5,5-bis(ethylenedioxy)-8-octanol

: 488-10-8
cis-jasmone

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / PCC / CH₂Cl₂ / 4 h / Ambient temperature

2: 80 percent / toluene / 8 h / Ambient temperature

3: 96 percent / aq. HCl / 2 h / 50 °C

4: 91 percent / aq. KOH / ethanol / 2 h / Heating

With hydrogenchloride; potassium hydroxide; pyridinium chlorochromate; In ethanol; dichloromethane; toluene;