(6-tert-butyl-5-methoxy-2-methyl-4-phenyl-1H-inden-1-yl)(chloro)dimethylsilane

Base Information

Chemical Name:(6-tert-butyl-5-methoxy-2-methyl-4-phenyl-1H-inden-1-yl)(chloro)dimethylsilane
CAS No.:1417536-78-7
Molecular Formula:C₂₃H₂₉ClOSi
Molecular Weight:385.021
Hs Code.:

Synonyms:(6-tert-butyl-5-methoxy-2-methyl-4-phenyl-1H-inden-1-yl)(chloro)dimethylsilane

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Chemical Property of (6-tert-butyl-5-methoxy-2-methyl-4-phenyl-1H-inden-1-yl)(chloro)dimethylsilane

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Technology Process of (6-tert-butyl-5-methoxy-2-methyl-4-phenyl-1H-inden-1-yl)(chloro)dimethylsilane

There total 5 articles about (6-tert-butyl-5-methoxy-2-methyl-4-phenyl-1H-inden-1-yl)(chloro)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 5-(tert-butyl)-6-methoxy-2-methyl-7-phenyl-1H-indene

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 1417536-78-7
(6-tert-butyl-5-methoxy-2-methyl-4-phenyl-1H-inden-1-yl)(chloro)dimethylsilane

Guidance literature:: 5-(tert-butyl)-6-methoxy-2-methyl-7-phenyl-1H-indene; With n-butyllithium; In tetrahydrofuran; hexane; toluene; at -20 - 60 ℃; for 16h;

dimethylsilicon dichloride; In tetrahydrofuran; hexane; toluene; at 60 ℃; for 1h;

Reference yield:

: 952516-22-2
6-tert-butyl-5-methoxy-2-methyl-1-indanone

: 1417536-78-7
(6-tert-butyl-5-methoxy-2-methyl-4-phenyl-1H-inden-1-yl)(chloro)dimethylsilane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate trihydrate; tetraethylammonium iodide; bromine / dichloromethane; water / 1.08 h / 5 °C

2.1: sodium carbonate; palladium diacetate; triphenylphosphine / water; 1,2-dimethoxyethane / 12 h / Reflux

3.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 2.5 h / 5 °C

4.1: n-butyllithium / tetrahydrofuran; toluene; hexane / 16 h / -20 - 60 °C

4.2: 1 h / 60 °C

With sodium tetrahydroborate; n-butyllithium; tetraethylammonium iodide; bromine; palladium diacetate; sodium acetate trihydrate; sodium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; hexane; dichloromethane; water; toluene;

Reference yield:

: 952516-23-3
4-bromo-6-tert-butyl-5-methoxy-2-methyl-1-indanone

: 1417536-78-7
(6-tert-butyl-5-methoxy-2-methyl-4-phenyl-1H-inden-1-yl)(chloro)dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate; palladium diacetate; triphenylphosphine / water; 1,2-dimethoxyethane / 12 h / Reflux

2.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 2.5 h / 5 °C

3.1: n-butyllithium / tetrahydrofuran; toluene; hexane / 16 h / -20 - 60 °C

3.2: 1 h / 60 °C

With sodium tetrahydroborate; n-butyllithium; palladium diacetate; sodium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; hexane; water; toluene;