(S,Z)-1-(1-benzyl-1H-pyrrol-2-yl)-2-benzylidene-3-(2-oxo-4-phenyloxazolidin-3-yl)propane-1,3-dione

Base Information

Chemical Name:(S,Z)-1-(1-benzyl-1H-pyrrol-2-yl)-2-benzylidene-3-(2-oxo-4-phenyloxazolidin-3-yl)propane-1,3-dione
CAS No.:1252612-26-2
Molecular Formula:C₃₀H₂₄N₂O₄
Molecular Weight:476.532
Hs Code.:

Synonyms:(S,Z)-1-(1-benzyl-1H-pyrrol-2-yl)-2-benzylidene-3-(2-oxo-4-phenyloxazolidin-3-yl)propane-1,3-dione

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Chemical Property of (S,Z)-1-(1-benzyl-1H-pyrrol-2-yl)-2-benzylidene-3-(2-oxo-4-phenyloxazolidin-3-yl)propane-1,3-dione

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Technology Process of (S,Z)-1-(1-benzyl-1H-pyrrol-2-yl)-2-benzylidene-3-(2-oxo-4-phenyloxazolidin-3-yl)propane-1,3-dione

There total 1 articles about (S,Z)-1-(1-benzyl-1H-pyrrol-2-yl)-2-benzylidene-3-(2-oxo-4-phenyloxazolidin-3-yl)propane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 51491-77-1
1-benzyl-1H-pyrrole-2-carbonyl chloride

: 192203-75-1
(4S)-3-(3-phenyl-2-propyonyl)-4-phenyloxazolidin-2-one

: 1252612-26-2
(S,Z)-1-(1-benzyl-1H-pyrrol-2-yl)-2-benzylidene-3-(2-oxo-4-phenyloxazolidin-3-yl)propane-1,3-dione

Guidance literature:: (4S)-3-(3-phenyl-2-propyonyl)-4-phenyloxazolidin-2-one; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride; In tetrahydrofuran; Inert atmosphere;

1-benzyl-1H-pyrrole-2-carbonyl chloride; With copper(l) chloride; In tetrahydrofuran; at 18 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo100736p

Reference yield: 81.0%

: 1252612-26-2
(S,Z)-1-(1-benzyl-1H-pyrrol-2-yl)-2-benzylidene-3-(2-oxo-4-phenyloxazolidin-3-yl)propane-1,3-dione

: 1252612-53-5
(S)-3-[(4S,5S)-1-benzyl-6-oxo-4-phenyl-1,4,5,6-tetrahydrocyclopenta[b]pyrrole-5-carbonyl]-4-phenyloxazolidin-2-one

: 1252612-55-7
(S)-3-[(4R,5R)-1-benzyl-6-oxo-4-phenyl-1,4,5,6-tetrahydrocyclopenta[b]pyrrole-5-carbonyl]-4-phenyloxazolidin-2-one

Guidance literature:: With methanesulfonic acid; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1021/jo100736p

Reference yield: 51.0%

: 1252612-26-2
(S,Z)-1-(1-benzyl-1H-pyrrol-2-yl)-2-benzylidene-3-(2-oxo-4-phenyloxazolidin-3-yl)propane-1,3-dione

: 1252612-54-6
(S)-3-[(4R,5S)-1-benzyl-6-oxo-4-phenyl-1,4,5,6-tetrahydrocyclopenta[b]pyrrole-5-carbonyl]-4-phenyloxazolidin-2-one

: 1252612-53-5
(S)-3-[(4S,5S)-1-benzyl-6-oxo-4-phenyl-1,4,5,6-tetrahydrocyclopenta[b]pyrrole-5-carbonyl]-4-phenyloxazolidin-2-one

: 1252612-52-4
(S)-3-[(4S,5R)-1-benzyl-6-oxo-4-phenyl-1,4,5,6-tetrahydrocyclopenta[b]pyrrole-5-carbonyl]-4-phenyloxazolidin-2-one

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; for 4h; Inert atmosphere; Reflux;
DOI:10.1021/jo100736p