C₂₃H₂₉NO₆S

Base Information

Chemical Name:C₂₃H₂₉NO₆S
CAS No.:1330744-83-6
Molecular Formula:C₂₃H₂₉NO₆S
Molecular Weight:447.552
Hs Code.:

C<sub>23</sub>H<sub>29</sub>NO<sub>6</sub>S

Synonyms:C₂₃H₂₉NO₆S

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Chemical Property of C₂₃H₂₉NO₆S

Chemical Property:

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Technology Process of C₂₃H₂₉NO₆S

There total 10 articles about C₂₃H₂₉NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1330744-81-4
C₂₄H₂₉NO₈S

: 1268460-36-1
narseronine

: 1330744-83-6
C₂₃H₂₉NO₆S

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimedone; In tetrahydrofuran; at 18 ℃; for 0.17h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.06.050

Reference yield:

: 1175589-00-0
C₁₁H₁₄BrNO₂

: 1330744-83-6
C₂₃H₂₉NO₆S

Guidance literature:: Multi-step reaction with 9 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂

2.1: hydrogen / 45004.5 Torr

3.1: pyridine

4.1: lithium hexamethyldisilazane

5.1: acetic acid / water / 0.6 h / 50 °C

5.2: -78 °C

5.3: Cooling with ice

6.1: silver(l) oxide / acetonitrile / 12 h / Reflux

7.1: sodium hydroxide / tetrahydrofuran; water / 0.5 h / 18 °C

8.1: oxalyl dichloride / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

8.2: 1 h / -78 °C / Inert atmosphere

8.3: -78 - 0 °C / Inert atmosphere

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimedone / tetrahydrofuran / 0.17 h / 18 °C / Inert atmosphere

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; oxalyl dichloride; hydrogen; dimedone; acetic acid; sodium hydroxide; silver(l) oxide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; acetonitrile; 1.1: Suzuki-Miyaura cross-coupling / 6.1: Irvine-Purdie methylation / 8.1: Swern oxidation / 8.2: Swern oxidation / 8.3: Swern oxidation;
DOI:10.1016/j.tetlet.2011.06.050

Reference yield:

: 1175588-94-9
C₁₁H₁₄BrNO₃

: 1330744-83-6
C₂₃H₂₉NO₆S

Guidance literature:: Multi-step reaction with 10 steps

1.1: carbon disulfide; sodium hydride

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂

3.1: hydrogen / 45004.5 Torr

4.1: pyridine

5.1: lithium hexamethyldisilazane

6.1: acetic acid / water / 0.6 h / 50 °C

6.2: -78 °C

6.3: Cooling with ice

7.1: silver(l) oxide / acetonitrile / 12 h / Reflux

8.1: sodium hydroxide / tetrahydrofuran; water / 0.5 h / 18 °C

9.1: oxalyl dichloride / dichloromethane / 0.25 h / -78 °C / Inert atmosphere

9.2: 1 h / -78 °C / Inert atmosphere

9.3: -78 - 0 °C / Inert atmosphere

10.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimedone / tetrahydrofuran / 0.17 h / 18 °C / Inert atmosphere

With pyridine; carbon disulfide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; oxalyl dichloride; hydrogen; sodium hydride; dimedone; acetic acid; sodium hydroxide; silver(l) oxide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; acetonitrile; 1.1: Barton-McCombie deoxygenation / 1.2: Barton-McCombie deoxygenation / 1.3: Barton-McCombie deoxygenation / 2.1: Suzuki-Miyaura cross-coupling / 7.1: Irvine-Purdie methylation / 9.1: Swern oxidation / 9.2: Swern oxidation / 9.3: Swern oxidation;
DOI:10.1016/j.tetlet.2011.06.050