benzyl methyl N,N-diisopropylphosphoramidite

Base Information

Chemical Name:benzyl methyl N,N-diisopropylphosphoramidite
CAS No.:173170-93-9
Molecular Formula:C₁₄H₂₄NO₂P
Molecular Weight:269.324
Hs Code.:

Synonyms:benzyl methyl N,N-diisopropylphosphoramidite

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Chemical Property of benzyl methyl N,N-diisopropylphosphoramidite

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Technology Process of benzyl methyl N,N-diisopropylphosphoramidite

There total 3 articles about benzyl methyl N,N-diisopropylphosphoramidite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 86030-43-5
N,N-diisopropylmethylphosphonamidic chloride

: 100-51-6,185532-71-2
benzyl alcohol

: 173170-93-9
benzyl methyl N,N-diisopropylphosphoramidite

Guidance literature:: With triethylamine; In diethyl ether; for 12h; Ambient temperature;
DOI:10.1139/cjc-76-6-836

Reference yield:

: 108-18-9
diisopropylamine

: 173170-93-9
benzyl methyl N,N-diisopropylphosphoramidite

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 2 h / Ambient temperature

2: N,N-diisopropylethylamine / 3 h / -20 - 20 °C

With N-ethyl-N,N-diisopropylamine; In diethyl ether;
DOI:10.1021/ja00154a017

Reference yield:

: 108-18-9
diisopropylamine

: 173170-93-9
benzyl methyl N,N-diisopropylphosphoramidite

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / Et₃N / diethyl ether / 12 h / Ambient temperature

2: 86 percent / Et₃N / diethyl ether / 12 h / Ambient temperature

With triethylamine; In diethyl ether;
DOI:10.1139/cjc-76-6-836