2-(5-(4-(methylsulfonyl)phenyl)-4-(4-(trifluoromethyl)phenyl)-4H-1,2,4-triazol-3-ylthio)acetaldehyde oxime

Base Information

Chemical Name:2-(5-(4-(methylsulfonyl)phenyl)-4-(4-(trifluoromethyl)phenyl)-4H-1,2,4-triazol-3-ylthio)acetaldehyde oxime
CAS No.:1579939-42-6
Molecular Formula:C₁₈H₁₅F₃N₄O₃S₂
Molecular Weight:456.469
Hs Code.:

Synonyms:2-(5-(4-(methylsulfonyl)phenyl)-4-(4-(trifluoromethyl)phenyl)-4H-1,2,4-triazol-3-ylthio)acetaldehyde oxime

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Chemical Property of 2-(5-(4-(methylsulfonyl)phenyl)-4-(4-(trifluoromethyl)phenyl)-4H-1,2,4-triazol-3-ylthio)acetaldehyde oxime

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Technology Process of 2-(5-(4-(methylsulfonyl)phenyl)-4-(4-(trifluoromethyl)phenyl)-4H-1,2,4-triazol-3-ylthio)acetaldehyde oxime

There total 5 articles about 2-(5-(4-(methylsulfonyl)phenyl)-4-(4-(trifluoromethyl)phenyl)-4H-1,2,4-triazol-3-ylthio)acetaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.1%

: 130111-04-5
2-bromoacetaldehyde oxime

: 1579939-40-4
C₁₆H₁₂F₃N₃O₂S₂

: 1579939-42-6
2-(5-(4-(methylsulfonyl)phenyl)-4-(4-(trifluoromethyl)phenyl)-4H-1,2,4-triazol-3-ylthio)acetaldehyde oxime

Guidance literature:: C₁₆H₁₂F₃N₃O₂S₂; With potassium carbonate; In acetone; at 50 ℃; for 0.5h;

2-bromoacetaldehyde oxime; In acetone; for 3h; Reflux;
DOI:10.1039/c3ob41936c

Reference yield:

: 22821-70-1
methyl 4-(methanesulfonyl)benzoate

: 1579939-42-6
2-(5-(4-(methylsulfonyl)phenyl)-4-(4-(trifluoromethyl)phenyl)-4H-1,2,4-triazol-3-ylthio)acetaldehyde oxime

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / ethanol / 6 h / Reflux

2.1: ethanol / 5 h / Reflux

3.1: sodium hydroxide / methanol / 2 h / Reflux

3.2: pH 2

4.1: potassium carbonate / acetone / 0.5 h / 50 °C

4.2: 3 h / Reflux

With potassium carbonate; hydrazine hydrate; sodium hydroxide; In methanol; ethanol; acetone;
DOI:10.1039/c3ob41936c

Reference yield:

: 4052-30-6
4-methylsulfonylbenzoic acid

: 1579939-42-6
2-(5-(4-(methylsulfonyl)phenyl)-4-(4-(trifluoromethyl)phenyl)-4H-1,2,4-triazol-3-ylthio)acetaldehyde oxime

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C

2.1: hydrazine hydrate / ethanol / 6 h / Reflux

3.1: ethanol / 5 h / Reflux

4.1: sodium hydroxide / methanol / 2 h / Reflux

4.2: pH 2

5.1: potassium carbonate / acetone / 0.5 h / 50 °C

5.2: 3 h / Reflux

With potassium carbonate; hydrazine hydrate; sodium hydroxide; In methanol; ethanol; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c3ob41936c