1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride

Base Information

Chemical Name:1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride
CAS No.:1620922-81-7
Molecular Formula:C₄₅H₇₇N₂O₈S₂Si₂*Cl
Molecular Weight:929.871
Hs Code.:

Synonyms:1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride

Suppliers and Price of 1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride

There total 4 articles about 1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 14814-09-6
3-Mercaptopropyltriethoxysilane

: 1620922-77-1
1,3-bis[4-(3-butenyloxy)-2,6-dimethylphenyl]imidazolium chloride

: 1620922-81-7
1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride

Guidance literature:: With 2,2-dimethoxy-2-phenylacetophenone; In ethanol; for 24h; Inert atmosphere; Schlenk technique; Irradiation;
DOI:10.1002/adsc.201300903

Reference yield:

: 3096-70-6
3,5-dimethyl-4-aminophenol

: 1620922-81-7
1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: formic acid / ethanol / 8 h / Inert atmosphere; Schlenk technique; Heating

2.1: potassium carbonate; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 48 h / Inert atmosphere; Schlenk technique; Reflux

3.1: toluene / 80 °C / Inert atmosphere; Schlenk technique

3.2: 2.75 h / Inert atmosphere; Schlenk technique; Heating

4.1: 2,2-dimethoxy-2-phenylacetophenone / ethanol / 24 h / Inert atmosphere; Schlenk technique; Irradiation

With formic acid; 2,2-dimethoxy-2-phenylacetophenone; tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; ethanol; toluene;
DOI:10.1002/adsc.201300903

Reference yield:

: 1620922-73-7
N,N’-bis[4-(3-butenyloxy)-2,6-dimethylphenyl]-1,4-diazabutadiene

: 1620922-81-7
1,3-bis[4-(4-{[3-(triethoxysilyl)propyl]thio}butyloxy)-2,6-dimethylphenyl]imidazolium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 80 °C / Inert atmosphere; Schlenk technique

1.2: 2.75 h / Inert atmosphere; Schlenk technique; Heating

2.1: 2,2-dimethoxy-2-phenylacetophenone / ethanol / 24 h / Inert atmosphere; Schlenk technique; Irradiation

With 2,2-dimethoxy-2-phenylacetophenone; In ethanol; toluene;
DOI:10.1002/adsc.201300903