Technology Process of C21H27N6O8P
There total 4 articles about C21H27N6O8P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium azide / N,N-dimethyl-formamide / 48 h / 120 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
3: 1-methyl-1H-imidazole / tetrahydrofuran / 20 °C / Inert atmosphere
With
1-methyl-1H-imidazole; lithium azide; tetrabutyl ammonium fluoride; acetic acid;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.05.051
- Guidance literature:
-
Multi-step reaction with 4 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 0.5 h / 80 °C / Inert atmosphere
2: lithium azide / N,N-dimethyl-formamide / 48 h / 120 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
4: 1-methyl-1H-imidazole / tetrahydrofuran / 20 °C / Inert atmosphere
With
1-methyl-1H-imidazole; lithium azide; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; acetic acid; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.ejmech.2011.05.051