1--1-tetraol

Base Information

• Chemical Name: 1--1-tetraol
• CAS No.: 145663-78-1
• Molecular Formula: C₁₇H₁₇ClO₂S
• Molecular Weight: 320.84

Synonyms:1--1-tetraol

Chemical Property of 1--1-tetraol

Chemical Property:

Purity/Quality:

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Technology Process of 1--1-tetraol

There total 1 articles about 1--1-tetraol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloromethyl phenyl sulfoxide (7205-94-9) + 3,4-dihydronaphthalene-1(2H)-one (529-34-0) → 1--1-tetraol (145663-78-1)

Guidance literature:

With lithium diisopropyl amide; Yield given. Multistep reaction; 1) THF, -60 deg C;

DOI:10.1016/S0040-4039(00)60867-5

Reference yield: 9.0%

1--1-tetraol (145663-78-1) → 1-(phenylsulfinyl)-2-benzosuberone (145663-85-0) + 2-(phenylsulfinyl)-1-benzosuberone (145663-84-9)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; at -75 - -40 ℃; for 1.5h;

DOI:10.1016/S0040-4039(00)60867-5

upstream raw materials:

chloromethyl phenyl sulfoxide

3,4-dihydronaphthalene-1(2H)-one

Downstream raw materials:

1-(phenylsulfinyl)-2-benzosuberone

2-(phenylsulfinyl)-1-benzosuberone

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