5-<(N,N-bis-2-<3,5-dimethylpyrazolyl>ethylamino)carbonyl>methyl-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

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Chemical Name:5-<(N,N-bis-2-<3,5-dimethylpyrazolyl>ethylamino)carbonyl>methyl-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene
CAS No.:217792-16-0
Molecular Formula:C₆₈H₅₉Br₄N₅O₁₃S₄
Molecular Weight:1602.12
Hs Code.:

Synonyms:5-<(N,N-bis-2-<3,5-dimethylpyrazolyl>ethylamino)carbonyl>methyl-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

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Chemical Property of 5-<(N,N-bis-2-<3,5-dimethylpyrazolyl>ethylamino)carbonyl>methyl-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

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Technology Process of 5-<(N,N-bis-2-<3,5-dimethylpyrazolyl>ethylamino)carbonyl>methyl-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

There total 4 articles about 5-<(N,N-bis-2-<3,5-dimethylpyrazolyl>ethylamino)carbonyl>methyl-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 85650-01-7
bis[2-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]amine

: 217792-09-1
5-(carboxymethyl)-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

: 217792-16-0
5-<(N,N-bis-2-<3,5-dimethylpyrazolyl>ethylamino)carbonyl>methyl-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; for 8h; Ambient temperature;
DOI:10.1021/jo981038l

Reference yield: 80.0%

: 85650-01-7
bis[2-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl]amine

: 217792-12-6
5-(chlorocarbonylmethyl)-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

: 217792-16-0
5-<(N,N-bis-2-<3,5-dimethylpyrazolyl>ethylamino)carbonyl>methyl-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

Guidance literature:: With triethylamine; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jo981038l

Reference yield:

: 172534-25-7
5-(cyanomethyl)-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

: 217792-16-0
5-<(N,N-bis-2-<3,5-dimethylpyrazolyl>ethylamino)carbonyl>methyl-25,26,27,28-tetrakis<<(p-bromophenyl)sulfonyl>oxy>calix<4>arene

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄ / H₂O; acetic acid / 16 h / Heating

2: 87 percent / DCC, HOBt / CH₂Cl₂ / 8 h / Ambient temperature

With sulfuric acid; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; water; acetic acid;
DOI:10.1021/jo981038l