(1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate

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Chemical Name:(1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate
CAS No.:499778-99-3
Molecular Formula:C₄₂H₆₁NO₁₂
Molecular Weight:771.946
Hs Code.:

(1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate

Synonyms:(1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate

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Chemical Property of (1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate

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Technology Process of (1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate

There total 6 articles about (1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₄₃H₆₂O₁₅S

: 499778-99-3
(1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate

Guidance literature:: With hydrogen; palladium dihydroxide; In methanol; at 20 ℃; for 1h; under 760 Torr;
DOI:10.1055/s-2002-34381

Reference yield:

: 321146-51-4
(1R,6R)-6-Hydroxy-4-{(2S,4S,6S)-8-[(2,2-dimethylpropanoyl)oxy]-2,4-isopropylidenedioxy-6-[(4-methoxybenzoyl)oxy]octyl}cyclohept-3-en-1-yl 4-methoxybenzoate

: 499778-99-3
(1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: aq. NMO / OsO₄ / acetone; CCl₄ / 2 h / 20 °C

2.1: Pb(OAc)4 / methanol / 0.33 h / 20 °C

3.1: Et₂BOMe / tetrahydrofuran / 1 h / 20 °C

3.2: NaBH₄ / methanol / 2 h / 0 °C

4.1: 82 percent / pyridinium toluene-4-sulfonate / acetone / 2 h / 0 °C

5.1: Et₃N / CH₂Cl₂ / 0.25 h / 0 °C

6.1: 100 percent / H₂ / Pd(OH)2/C / methanol / 1 h / 20 °C / 760 Torr

With lead(IV) acetate; N-methyl-2-indolinone; diethyl methoxy borane; hydrogen; pyridinium p-toluenesulfonate; triethylamine; palladium dihydroxide; osmium(VIII) oxide; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; acetone;
DOI:10.1055/s-2002-34381

Reference yield:

: 499778-95-9
C₃₉H₅₂O₁₃

: 499778-99-3
(1R)-3-amino-1-{[(4R,6S)-6-[{(4S,6S)-6-(2S)-4-(2,2-dimethyl-1-oxopropoxy)-2-[(4-methoxybenzoyl)oxy]butyl-2,2-dimethyl-1,3-dioxan-4-yl}methyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl}propyl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: Et₂BOMe / tetrahydrofuran / 1 h / 20 °C

1.2: NaBH₄ / methanol / 2 h / 0 °C

2.1: 82 percent / pyridinium toluene-4-sulfonate / acetone / 2 h / 0 °C

3.1: Et₃N / CH₂Cl₂ / 0.25 h / 0 °C

4.1: 100 percent / H₂ / Pd(OH)2/C / methanol / 1 h / 20 °C / 760 Torr

With diethyl methoxy borane; hydrogen; pyridinium p-toluenesulfonate; triethylamine; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1055/s-2002-34381