{1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-hydroxyethyl)imidazolidin-2-ylidene}benzenesulfonylacetonitrile

Base Information

Chemical Name:{1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-hydroxyethyl)imidazolidin-2-ylidene}benzenesulfonylacetonitrile
CAS No.:904678-81-5
Molecular Formula:C₂₂H₃₅N₃O₄SSi
Molecular Weight:465.689
Hs Code.:

Synonyms:{1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-hydroxyethyl)imidazolidin-2-ylidene}benzenesulfonylacetonitrile

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Chemical Property of {1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-hydroxyethyl)imidazolidin-2-ylidene}benzenesulfonylacetonitrile

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Technology Process of {1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-hydroxyethyl)imidazolidin-2-ylidene}benzenesulfonylacetonitrile

There total 1 articles about {1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-hydroxyethyl)imidazolidin-2-ylidene}benzenesulfonylacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.5%

: 58092-40-3
2-benzenesulfonyl-3,3-bis(methylsulfanyl)acrylonitrile

: 89031-84-5
3-(tert-butyldimethylsilyloxy)propyl bromide

: 904678-81-5
{1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-hydroxyethyl)imidazolidin-2-ylidene}benzenesulfonylacetonitrile

Guidance literature:: 2-benzenesulfonyl-3,3-bis(methylsulfanyl)acrylonitrile; 2-(2-Aminoethylamino)ethanol; With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 1h;

3-(tert-butyldimethylsilyloxy)propyl bromide; With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 23h;

3-(tert-butyldimethylsilyloxy)propyl bromide; With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 4.5h;

Reference yield: 16.4%

: 904678-81-5
{1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-hydroxyethyl)imidazolidin-2-ylidene}benzenesulfonylacetonitrile

: 765-38-8
2-methyl-1-pyrrolidine

: 904678-83-7
{1-[3-(tert-butyldimethylsilyloxy)propyl]-3-[2-(2-methylpyrrolidin-1-yl)ethyl]imidazolidin-2-ylidene} benzenesulfonylacetonitrile

Guidance literature:: {1-[3-(tert-butyldimethylsilyloxy)propyl]-3-(2-hydroxyethyl)imidazolidin-2-ylidene}benzenesulfonylacetonitrile; benzenesulfonyl chloride; With triethylamine; In dichloromethane; at 20 ℃; for 2h;

2-methyl-1-pyrrolidine; With potassium carbonate; sodium iodide; In 1,4-dioxane; at 80 ℃; for 24h;