C₂₃H₁₉BF₂N₂O₃

Base Information

Chemical Name:C₂₃H₁₉BF₂N₂O₃
CAS No.:1446260-37-2
Molecular Formula:C₂₃H₁₉BF₂N₂O₃
Molecular Weight:420.223
Hs Code.:

C<sub>23</sub>H<sub>19</sub>BF<sub>2</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₃H₁₉BF₂N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₁₉BF₂N₂O₃

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Technology Process of C₂₃H₁₉BF₂N₂O₃

There total 3 articles about C₂₃H₁₉BF₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1446260-36-1
C₂₃H₂₁BF₂N₂O₃

: 1446260-37-2
C₂₃H₁₉BF₂N₂O₃

Guidance literature:: With sodium sulfate; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3cc44539a

Reference yield:

: 1361018-77-0
3-bromo-4-(((tert-butyldimethylsilyl)oxy)methyl)benzaldehyde

: 1446260-37-2
C₂₃H₁₉BF₂N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; palladium diacetate; triphenylphosphine / acetonitrile / 18 h / Inert atmosphere; Reflux

2: piperidine; acetic acid / benzene / Reflux; Dean-Stark; Inert atmosphere

3: hydrogen fluoride / acetonitrile; water / 1 h / 20 °C / Inert atmosphere

4: pyridinium chlorochromate; sodium sulfate / dichloromethane / 1 h / 20 °C / Inert atmosphere

With piperidine; hydrogen fluoride; palladium diacetate; acetic acid; sodium sulfate; triethylamine; triphenylphosphine; pyridinium chlorochromate; In dichloromethane; water; acetonitrile; benzene; 2: |Knoevenagel Condensation;
DOI:10.1039/c3cc44539a

Reference yield:

: C₁₈H₂₆O₄Si

: 1446260-37-2
C₂₃H₁₉BF₂N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine; acetic acid / benzene / Reflux; Dean-Stark; Inert atmosphere

2: hydrogen fluoride / acetonitrile; water / 1 h / 20 °C / Inert atmosphere

3: pyridinium chlorochromate; sodium sulfate / dichloromethane / 1 h / 20 °C / Inert atmosphere

With piperidine; hydrogen fluoride; acetic acid; sodium sulfate; pyridinium chlorochromate; In dichloromethane; water; acetonitrile; benzene; 1: |Knoevenagel Condensation;
DOI:10.1039/c3cc44539a