4'-(11-[4-boronpinacolatephenylcarboxy]undecyloxy)-biphenyl-4-carbonitrile

Base Information

Chemical Name:4'-(11-[4-boronpinacolatephenylcarboxy]undecyloxy)-biphenyl-4-carbonitrile
CAS No.:1318805-01-4
Molecular Formula:C₃₇H₄₆BNO₅
Molecular Weight:595.587
Hs Code.:

Synonyms:4'-(11-[4-boronpinacolatephenylcarboxy]undecyloxy)-biphenyl-4-carbonitrile

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Chemical Property of 4'-(11-[4-boronpinacolatephenylcarboxy]undecyloxy)-biphenyl-4-carbonitrile

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Technology Process of 4'-(11-[4-boronpinacolatephenylcarboxy]undecyloxy)-biphenyl-4-carbonitrile

There total 3 articles about 4'-(11-[4-boronpinacolatephenylcarboxy]undecyloxy)-biphenyl-4-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 83577-78-0
4'-(11-hydroxyundecyloxy)-4-cyanobiphenyl

: 180516-87-4
4-carboxyphenylboronic acid pinacol ester

: 1318805-01-4
4'-(11-[4-boronpinacolatephenylcarboxy]undecyloxy)-biphenyl-4-carbonitrile

Guidance literature:: With dicyclohexylcarbodiimide; DMAP; In dichloromethane;
DOI:10.1039/c0nj00990c

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 1318805-01-4
4'-(11-[4-boronpinacolatephenylcarboxy]undecyloxy)-biphenyl-4-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetone / 18 h / Reflux

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 18 h / 20 °C

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; potassium iodide; In dichloromethane; acetone; 1: Williamson ether synthesis;
DOI:10.1039/c0nj00990c

Reference yield:

: 19812-93-2
4-Cyano-4'-hydroxybiphenyl

: 1318805-01-4
4'-(11-[4-boronpinacolatephenylcarboxy]undecyloxy)-biphenyl-4-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetone / 18 h / Reflux

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 18 h / 20 °C

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; potassium iodide; In dichloromethane; acetone; 1: Williamson ether synthesis;
DOI:10.1039/c0nj00990c