6-Methylpyridine-3-carbohydrazide

Base Information

• Chemical Name: 6-Methylpyridine-3-carbohydrazide
• CAS No.: 197079-25-7
• Molecular Formula: C7H9 N3 O
• Molecular Weight: 151.168
• DSSTox Substance ID: DTXSID80408843
• Wikidata: Q82214452
• Mol file: 197079-25-7.mol

Synonyms:197079-25-7;6-methylpyridine-3-carbohydrazide;6-Methylnicotinoyl hydrazide;6-methylnicotinohydrazide;6-Methyl-3-pyridinecarboxylic acid hydrazide;6-methylnicotinic acid hydrazide;MFCD01838565;3-Pyridinecarboxylicacid,6-methyl-,hydrazide(9CI);3-Pyridinecarboxylicacid, 6-methyl-, hydrazide;6-Methylnicotinoylhydrazide;Oprea1_645982;SCHEMBL1883198;6-methyl-nicotinic acid hydrazide;DTXSID80408843;WXHPYVNOEDALAS-UHFFFAOYSA-N;AKOS000147489;FS-5133;SB85924;6-Methyl-3-pyridinecarboxylicacidhydrazide;SY073938;CS-0312605;3-pyridinecarboxylic acid,6-methyl-,hydrazide;EN300-1168274

Chemical Property of 6-Methylpyridine-3-carbohydrazide

Chemical Property:

• PSA: 71.50000
• LogP: 1.26860
• XLogP3: -0.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 151.074561919
• Heavy Atom Count: 11
• Complexity: 149

Purity/Quality:

98%min ^*data from raw suppliers

6-Methyl-3-pyridinecarboxylic acid hydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=NC=C(C=C1)C(=O)NN

Technology Process of 6-Methylpyridine-3-carbohydrazide

There total 4 articles about 6-Methylpyridine-3-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Methyl 6-methylnicotinate (5470-70-2) → 6-methylpyridine-3-carbohydrazide (197079-25-7)

Guidance literature:

With hydrazine hydrate; In ethanol; for 16h; Reflux;

Reference yield:

5-ethyl-2-methyl-pyridine (104-90-5) → 6-methylpyridine-3-carbohydrazide (197079-25-7)

Guidance literature:

Multi-step reaction with 2 steps

1: nitric acid; sulfuric acid / 150 °C

2: hydrazine hydrate / ethanol / 2 h / Reflux

With sulfuric acid; nitric acid; hydrazine hydrate; In ethanol;

DOI:10.1016/j.ejmech.2013.07.019

Reference yield:

ethyl 6-methylnicotinate (21684-59-3) → 6-methylpyridine-3-carbohydrazide (197079-25-7)

Guidance literature:

With hydrazine hydrate;

upstream raw materials:

ethyl 6-methylnicotinate

Methyl 6-methylnicotinate

5-ethyl-2-methyl-pyridine

Downstream raw materials:

6-methyl-nicotinoyl azide

C₁₆H₁₄BrN₃O₂S

C₁₄H₁₂BrN₃O

C₁₆H₁₄FN₃O₂S

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